A gold nanoring stacked array substrate with surface-enhanced Raman scattering and its preparation method
A surface-enhanced Raman and array substrate technology, which is used in Raman scattering, photolithography on patterned surfaces, opto-mechanical equipment, etc., can solve the problem of not being able to meet the requirements of large area, uniformity and high enhanced signal of SERS substrates at the same time. , it is difficult to control the particle spacing and other problems, to achieve the effect of easy large-area preparation, strong Raman signal enhancement effect, and easy control of the period
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Embodiment 1
[0041] (1) cleaning the substrate, with a thickness of 1.2 mm single-sided polished silicon as the substrate material 30, its reflectivity in the visible light range is higher than 80%, it is placed in acetone, absolute ethanol, deionized water for ultrasonic cleaning, Blow dry with high-purity nitrogen for 100-150s each time, select positive photoresist 29, the type is AR-P3740 for glue coating, the resolution is 0.5μm, the rotation speed of the homogenizer is 4000r / min, and the thickness of the glue is 1.5μm, then put it on a hot plate, pre-baked at 100°C, the pre-baked time is 1min, take it off, and place it in dark conditions, such as image 3 The gluing process in is shown in 26;
[0042] (2) Exposure is performed using a four-beam laser interference lithography system. The four-beam interference system generates modulation by controlling the incident angle. A 360nm semiconductor laser is the light source for the system, such as figure 2 As shown, the beam emitted by th...
Embodiment 2
[0047] (1) cleaning the substrate, with a thickness of 1.2 mm single-sided polished silicon as the substrate material 30, its reflectivity in the visible light range is higher than 80%, it is placed in acetone, absolute ethanol, deionized water for ultrasonic cleaning, Blow dry with high-purity nitrogen for 100-150s each time, select positive photoresist 29, the type is AR-P3740 for glue coating, the resolution is 0.5μm, the rotation speed of the homogenizer is 4000r / min, and the thickness of the glue is 1.5μm, then put it on a hot plate, pre-baked at 100°C, the pre-baked time is 1min, take it off, and place it in dark conditions, such as image 3 The gluing process in is shown in 26;
[0048] (2) Use a non-modulating three-beam interference lithography system for exposure. The incident angles of the first beam and the second beam of coherent light in the three beams are both 14°. At the same time, the spatial angles of the first beam of coherent light are respectively is 0°,...
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