Method for preparing ceramic filters with hot pressure casting process
A ceramic filter, hot pressure injection technology, applied in membrane filters, chemical instruments and methods, separation methods, etc., can solve the problems of poor pore distribution uniformity, low porosity, and inability to achieve fine particle filtration, and achieve pore distribution. Ease of control, the effect of reducing the sintering temperature
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Embodiment 1
[0026] (1) Preparation of high-performance alumina composite powder,
[0027] ① 1000g of alumina powder with a particle size of 5 microns is mixed with 10g, 10g, 20g, 10g, 10g, and 20g of oxides of calcium, magnesium, iron, potassium, sodium, and silicon respectively as auxiliary materials for 2 hours to obtain Aluminum oxide powder.
[0028] ② Add 500g of wood chips with a particle size of 400 microns as a pore-forming agent to the alumina powder, and stir and mix at normal temperature and pressure to obtain alumina composite powder.
[0029] (2) Preparation of slurry
[0030] ① Mix alumina composite powder and paraffin in a ratio of 20 / 200, heat at 60°C, and mechanically stir continuously for 12 hours to prepare a slurry with good fluidity and uniform mixing.
[0031] ② Vacuum defoaming. Mix the homogeneous slurry and remove the air bubbles in the slurry under vacuum conditions.
[0032] (3) injection molding
[0033] The prepared slurry is injected into a square sheet ...
Embodiment 2
[0040] (1) Preparation of high-performance alumina composite powder,
[0041] ① Take 300g of alumina with a particle size of 5 microns, 700g of alumina with a particle size of 50 microns, and 20g, 20g, 10g, 10g, 10g, and 20g of calcium, magnesium, iron, potassium, sodium, and silicon oxide auxiliary materials respectively. The dry powder was ball milled and mixed for 2 hours to obtain alumina powder.
[0042] ②Add 200g of carbon powder with a particle size of 5 microns and 300g of carbon powder with a particle size of 30 microns as pore-forming agents to the alumina powder, and stir and mix at normal temperature and pressure to obtain alumina composite powder.
[0043] (2) Preparation of slurry
[0044] ① Mix alumina composite powder and paraffin in a ratio of 25 / 200, heat at 80°C, and keep stirring mechanically for 24 hours to prepare a slurry with good fluidity and uniform mixing.
[0045] ② Vacuum defoaming. Mix the homogeneous slurry and remove the air bubbles in the sl...
Embodiment 3
[0054] (1) Preparation of high-performance alumina composite powder,
[0055] ① Take 300g of alumina with a particle size of 5 microns, 100g of alumina with a particle size of 50 microns, and 700g of alumina with a particle size of 100 microns, and the oxide auxiliary materials of calcium, magnesium, iron, potassium, sodium, and silicon as 15g, 20g, 10g, 10g, and 10g, respectively. , 15 g were ball milled and mixed for 2 hours to obtain alumina powder.
[0056] ② Add 700 g of ammonium salt with a particle size of 500 microns as a pore-forming agent to the alumina powder, and stir and mix at normal temperature and pressure to obtain alumina composite powder.
[0057] (2) Preparation of slurry
[0058]① Mix alumina composite powder and paraffin wax according to the ratio of 60 / 200, heat at 50°C, and mechanically stir continuously for 24 hours to prepare a slurry with good fluidity and uniform mixing.
[0059] ② Vacuum defoaming. Mix the homogeneous slurry and remove the air b...
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