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Method for preparing ceramic filters with hot pressure casting process

A ceramic filter, hot pressure injection technology, applied in membrane filters, chemical instruments and methods, separation methods, etc., can solve the problems of poor pore distribution uniformity, low porosity, and inability to achieve fine particle filtration, and achieve pore distribution. Ease of control, the effect of reducing the sintering temperature

Inactive Publication Date: 2018-06-19
辽宁法库陶瓷工程技术研究中心
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Porous ceramics prepared by extrusion molding have uniform pore shape and pore size distribution, but are not suitable for preparing porous ceramics with a pore size of less than 1mm; traditional methods of adding pore-forming agents to prepare porous ceramics have poor pore distribution uniformity and are not suitable for preparation Products with high porosity; the foaming method adds organic or inorganic pore-forming agents, generates volatile gases through physical or chemical reactions to produce foam, and is made into porous ceramics after drying and sintering, which is not suitable for the preparation of products with through-pore structures; The organic foam impregnation method prepares porous ceramics, and its pore size mainly depends on the pore size of the organic foam, and its products cannot achieve the filtration of tiny particles; the sol-gel method obtains pores through phase change or chemical reaction, and the pore size is nanoscale. low porosity
Due to the limitations of the above process, the obtained pore size and porosity are limited to a certain range, and it is difficult to prepare porous ceramic filters with micron pore size, high porosity, high strength and specific shape.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0026] (1) Preparation of high-performance alumina composite powder,

[0027] ① 1000g of alumina powder with a particle size of 5 microns is mixed with 10g, 10g, 20g, 10g, 10g, and 20g of oxides of calcium, magnesium, iron, potassium, sodium, and silicon respectively as auxiliary materials for 2 hours to obtain Aluminum oxide powder.

[0028] ② Add 500g of wood chips with a particle size of 400 microns as a pore-forming agent to the alumina powder, and stir and mix at normal temperature and pressure to obtain alumina composite powder.

[0029] (2) Preparation of slurry

[0030] ① Mix alumina composite powder and paraffin in a ratio of 20 / 200, heat at 60°C, and mechanically stir continuously for 12 hours to prepare a slurry with good fluidity and uniform mixing.

[0031] ② Vacuum defoaming. Mix the homogeneous slurry and remove the air bubbles in the slurry under vacuum conditions.

[0032] (3) injection molding

[0033] The prepared slurry is injected into a square sheet ...

Embodiment 2

[0040] (1) Preparation of high-performance alumina composite powder,

[0041] ① Take 300g of alumina with a particle size of 5 microns, 700g of alumina with a particle size of 50 microns, and 20g, 20g, 10g, 10g, 10g, and 20g of calcium, magnesium, iron, potassium, sodium, and silicon oxide auxiliary materials respectively. The dry powder was ball milled and mixed for 2 hours to obtain alumina powder.

[0042] ②Add 200g of carbon powder with a particle size of 5 microns and 300g of carbon powder with a particle size of 30 microns as pore-forming agents to the alumina powder, and stir and mix at normal temperature and pressure to obtain alumina composite powder.

[0043] (2) Preparation of slurry

[0044] ① Mix alumina composite powder and paraffin in a ratio of 25 / 200, heat at 80°C, and keep stirring mechanically for 24 hours to prepare a slurry with good fluidity and uniform mixing.

[0045] ② Vacuum defoaming. Mix the homogeneous slurry and remove the air bubbles in the sl...

Embodiment 3

[0054] (1) Preparation of high-performance alumina composite powder,

[0055] ① Take 300g of alumina with a particle size of 5 microns, 100g of alumina with a particle size of 50 microns, and 700g of alumina with a particle size of 100 microns, and the oxide auxiliary materials of calcium, magnesium, iron, potassium, sodium, and silicon as 15g, 20g, 10g, 10g, and 10g, respectively. , 15 g were ball milled and mixed for 2 hours to obtain alumina powder.

[0056] ② Add 700 g of ammonium salt with a particle size of 500 microns as a pore-forming agent to the alumina powder, and stir and mix at normal temperature and pressure to obtain alumina composite powder.

[0057] (2) Preparation of slurry

[0058]① Mix alumina composite powder and paraffin wax according to the ratio of 60 / 200, heat at 50°C, and mechanically stir continuously for 24 hours to prepare a slurry with good fluidity and uniform mixing.

[0059] ② Vacuum defoaming. Mix the homogeneous slurry and remove the air b...

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Abstract

The invention relates to a method for preparing ceramic filters with a hot pressure casting process. The method comprises steps as follows: alumina powder with proper grain size distribution and paraffin are mixed in a certain ratio, one or more pore-forming agents such as carbon powder, wood chips, aluminum salt, titanium salt, magnesium salt, sodium salt, lanthanum salt, cerium salt and the likeare added according to the size and distribution of required pores, and alumina slurry is configured. Under certain pressure, the slurry is injected into a mold meeting the shape requirement for forming, and various special-shaped filter bodies meeting the requirements are prepared; the bodies are subjected to removal burning, the pore-forming agents are removed, and porous bodies are obtained; the porous bodies are sintered at the high temperature, and the special-shaped alumina ceramic filters are obtained. In the whole process, no special mechanical equipment is required, the pore size anddistribution and the shapes of the filters are controllable, and the method is an ideal process for preparing high-porosity, high-strength and special-shaped ceramic filters.

Description

technical field [0001] The invention relates to a method for preparing a ceramic filter by a hot pressure injection process, Background technique [0002] With the development of society, the environmental pressure is becoming more and more serious, which leads to the gradual increase of the requirements for filtration devices in various fields. Taking metallurgy, machinery, chemical industry, electric power and other industries as examples, the high-temperature dust-laden gas discharged from various industrial furnaces not only has a high temperature (500-1200°C), but also contains a large amount of dust (5-30μm) and corrosion-reducing properties. Gas is one of the main factors causing environmental pollution. Under high temperature conditions, due to the large change in the viscous force of the dust-laden gas, the humidity drops sharply, and the agglomeration of fine particles is greatly reduced, so it is more difficult to separate the particles. The bag type dust collec...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B38/06C04B38/02C04B35/10B28B13/02B28B13/06B28B3/00B01D39/20
CPCB01D39/2093B01D2239/10B28B3/00B28B13/02B28B13/06C04B35/10C04B38/02C04B38/068C04B2235/3201C04B2235/3206C04B2235/3208C04B2235/3272C04B2235/3418C04B2235/96C04B38/0058C04B38/0074C04B38/0051C04B38/0054
Inventor 岳鑫杨殿来许壮志胡金玲张莹莹
Owner 辽宁法库陶瓷工程技术研究中心
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