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Plant polysaccharide heat insulation aerogel material and preparation method

A thermal insulation and aerogel technology, which is applied to the preparation of konjac polysaccharide thermal insulation aerogel and the field of konjac polysaccharide thermal insulation aerogel, can solve the problems of environmental pollution, pollute the environment, easy to burn, etc. The effect of improving mechanical properties

Active Publication Date: 2018-07-17
武汉锐致科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, most of the materials used for thermal insulation walls on the market are organic thermal insulation materials, mostly polystyrene boards and polyurethane materials. EPS has relatively low thermal conductivity, and has excellent characteristics such as waterproof and high strength, so it has a wide range of applications. However, organic thermal insulation materials also have many defects: these materials will pollute the environment during the production and processing of raw materials, cost high, pollute the environment, waste resources and are extremely flammable and easy to cause fires
However, the raw materials of current insulation materials are non-renewable, and most of the materials after production are non-degradable. Therefore, it is difficult to decompose when the materials are discarded after use. Some toxic gases are produced during combustion, which pollutes the environment. human bodily harm
In recent years, airgel prepared by supercritical drying method has appeared, which has excellent high temperature resistance and has been used in the aerospace field. However, most of the aerogels currently use petroleum as a precursor. Due to excessive exploitation by humans, Petroleum resources are limited, the production process is complicated, and the cost is high. The resources are limited, the cost is high, the toxicity is high, and the degradation is difficult

Method used

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  • Plant polysaccharide heat insulation aerogel material and preparation method
  • Plant polysaccharide heat insulation aerogel material and preparation method
  • Plant polysaccharide heat insulation aerogel material and preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0052] A kind of konjac polysaccharide thermal insulation aerogel, it is made of the raw material of following weight or volume:

[0053]

[0054]

[0055] A method for preparing konjac polysaccharide thermal insulation airgel, characterized in that it is prepared according to the following steps:

[0056] (1) Chitosan was dissolved in 50mL 1v / v% acetic acid solution, stirred at room temperature for 30min to obtain solution A;

[0057] (2) Take a certain amount of deionized water and add glycerin, under the condition of mechanical stirring at 800rpm, then add starch, konjac glucomannan, auxiliary glue, straw, nano-calcium carbonate, and stir quickly to obtain solution B;

[0058] (3) Mix solution A and solution B to obtain solution C, and stir solution C at 60°C for 3.5 hours to obtain a transparent viscous gel;

[0059] (4) Pour the stirred transparent viscous gel homogeneously into a mold and cool it into a gel;

[0060] (5) Pre-freezing at -30°C for 24 hours;

[00...

Embodiment 2-8

[0062] Embodiment 2-8: According to the raw material components in Table 1, according to the process parameters in Table 2, the preparation steps are the same as those in Example 1. The performance indexes of the prepared konjac polysaccharide thermal insulation airgel are shown in Table 3.

[0063] Table 1: The raw material composition table of embodiment

[0064]

[0065]

[0066] Table 2. Process parameter list

[0067]

Example 2

Example 3

Example 4

Example 5

Example 6

Example 7

Example 8

Solution A stirring time (min)

45

30

35

55

50

60

30

speed(rpm)

700

600

800

900

1200

1500

400

Stirring temperature of solution C (°C)

75

70

75

80

85

90

60

Solution C stirring time (h)

0.8

0.5

1

1.5

2.5

3

0.5

Pre-freezing temperature (℃)

-15

-10

-20

-25

-45

-60

-12

Pre-freezing time (h)

8

6

10

...

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Abstract

The invention relates to a plant polysaccharide heat insulation aerogel material and a preparation method. The plant polysaccharide heat insulation aerogel material is composed of starch, konjac glucomannan, auxiliary glue, glycerin, straws, nano calcium carbonate, chitosan and acetic acid according to a certain ratio. The preparation method comprises the following steps: (1) dissolving chitosan into an acetic acid solution, and stirring at a room temperature to obtain a solution A; (2) adding glycerin into deionized water, adding starch, konjac glucomannan, auxiliary glue, straws and inorganic fillers, and uniformly stirring to obtain a solution B; (3) mixing the solution A and the solution B to obtain a solution C, and stirring the solution C under the condition of 60-90 DEG C so as to obtain transparent viscous gel; (4) homogenizing the stirred transparent viscous gel, pouring the viscous gel into a mold, and cooling into gel; (5) performing freeze drying. The aerogel is excellent in mechanical property, has a low heat conductivity coefficient and can be applied to building insulation boards, mobile house walls and refrigerator insulation layers. The raw materials and aerogel are biodegradable, and the whole production process is green and pollution-free.

Description

technical field [0001] The invention belongs to biopolymer-based airgel natural thermal insulation materials, and more specifically relates to a konjac polysaccharide thermal insulation aerogel, and also relates to a preparation method of the konjac polysaccharide thermal insulation aerogel. Background technique [0002] With the rapid development of modern society and economy, the ecological environment is deteriorating. Since the 1970s, after the Western oil crisis, human beings have begun to pay attention to energy conservation. The energy consumption in the construction field is large. One of the means of building energy conservation is to use building insulation materials, which can Reduce floor space and reduce energy consumption. At present, most of the materials used for thermal insulation walls on the market are organic thermal insulation materials, mostly polystyrene boards and polyurethane materials. EPS has relatively low thermal conductivity, and has excellent c...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08J9/26C08L3/02C08L5/02C08L97/02C08L5/08C08L5/00C08L89/00C08K13/02C08K5/053C08K5/09C08K3/26C08K3/36C08K3/34
CPCC08J9/26C08J2303/02C08J2405/00C08J2405/02C08J2405/08C08J2489/00C08J2497/02C08L3/02C08L2203/14C08L2205/02C08L2205/035C08L5/02C08L97/02C08L5/08C08L5/00C08L89/00C08K13/02C08K5/053C08K5/09C08K2003/265C08K3/36C08K3/346
Inventor 王亦欣黄静姜发堂
Owner 武汉锐致科技有限公司
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