Resin composition and polyimide film and circuit board using resin composition
A resin composition, polyimide film technology, applied in printed circuit parts, compounds of periodic table Group 5/15 elements, organic chemistry, etc. The circuit board cannot achieve high-frequency signal transmission impedance matching and other problems, and achieve the effects of excellent flame retardancy, improved heat resistance, and increased cross-linking density
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Embodiment 1
[0032] Add 4.8g of DOPO, 3.0g of p-aminoacetophenone, 4.8g of o-aminophenol, 0.19g of p-toluenesulfonic acid and 10g of dimethyl sulfoxide in the first reaction flask and stir to dissolve, then in a nitrogen atmosphere The chemical structural formula is prepared by heating at 100 degrees Celsius for 12 hours of the first product.
[0033] Add 1.0g of the first product, 0.7g of pyromellitic dianhydride, 6.8g of N-methylpyrrolidone and 3.4g of xylene in the second reaction flask and stir to dissolve, and then in a nitrogen atmosphere at 140 degrees Celsius Heated for 20 hours to reflux and remove water to prepare the chemical structural formula as of the second product.
[0034] In the third reaction flask, add 10g of the second product, 3.5g of 2-methacrylic anhydride, 0.1g of sodium acetate and 100g of N,N-dimethylacetamide and stir to dissolve, and then in a nitrogen atmosphere at 80 The chemical structural formula is prepared by heating at a temperature of 12 degrees Ce...
Embodiment 2
[0037] The pyromellitic dianhydride of described 0.7g in embodiment 1 is replaced with the 4 of 0.7g, and the 4'-oxygen diphthalic anhydride and other conditions are constant preparation chemical structural formula is modified polyimide polymer compound (II).
[0038] Add 100g modified polyimide macromolecular compound (II) successively in the reaction bottle, and the chemical structural formula that is 1 with the molar ratio of described modified polyimide macromolecular compound (II) is The epoxy resin and 100g of N,N-dimethylacetamide were stirred and dissolved to complete the resin composition. The viscosity of the resin composition is 40000cps.
Embodiment 3
[0040] The pyromellitic dianhydride of described 0.7g in embodiment 1 is replaced with 0.7g 3,4,3 ', 4'-biphenyltetracarboxylic dianhydride and other conditions are constant preparation chemical structural formula is modified polyimide polymer compound (III).
[0041] Add 100g modified polyimide macromolecular compound (III) successively in reaction flask, the chemical structural formula that is 1 with the molar ratio of described modified polyimide macromolecular compound (III) is: The epoxy resin and 100g of N,N-dimethylacetamide were stirred and dissolved to complete the resin composition. The viscosity of the resin composition is 48000cps.
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