Method for preparing novel thermal insulation material
A thermal insulation material and a new type of technology are applied in the field of preparation of new thermal insulation materials, which can solve the problems of restricting the wide application of nanoporous thermal insulation materials, complicated preparation process and high cost, and achieve the effects of enhanced temperature adsorption effect, high performance and low cost.
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Embodiment 1
[0024] A method for preparing a novel heat insulating material, comprising the following steps:
[0025] a. Mix the modified montmorillonite, inorganic fiber, silica and portland cement, introduce into the high mixer, stir and disperse for 40min at the speed of 800r / min, and obtain the base material;
[0026] b. Add nano-dispersion liquid to the base material, heat at 120°C and stir for 30 minutes, then add absolute ethanol, cool to 65°C, heat and stir for 10 minutes to obtain material 1;
[0027] c. Add silicon nitride powder, sodium dodecylbenzenesulfonate and activated carbon emulsion to material 1, stir at a speed of 300r / min for 20min, then add binder and opacifier, and stir to obtain a slurry;
[0028] d. Introduce the slurry into the mold, then place it in a vacuum drying oven, dry it at 80°C and a pressure of 3MPa for 2 hours, and then take it out for curing treatment to obtain the finished product.
[0029] The preparation method of the modified montmorillonite in st...
Embodiment 2
[0037] A method for preparing a novel heat insulating material, comprising the following steps:
[0038] a. Mix the modified montmorillonite, inorganic fiber, silica and portland cement, introduce into the high mixer, stir and disperse for 30min at the speed of 800r / min, and obtain the base material;
[0039] b. Add nano-dispersion liquid to the base material, heat at 90°C and stir for 30 minutes, then add absolute ethanol, cool down to 55°C, heat and stir for 10 minutes to obtain material 1;
[0040] c. Add silicon nitride powder, sodium dodecylbenzenesulfonate and activated carbon emulsion to material 1, stir at a speed of 200r / min for 20min, then add binder and opacifier, and stir to obtain a slurry;
[0041] d. Introduce the slurry into the mold, then place it in a vacuum drying oven, dry it at 70°C and a pressure of 3MPa for 2 hours, and then take it out for curing treatment to obtain the finished product.
[0042] The preparation method of the modified montmorillonite i...
Embodiment 3
[0050] A method for preparing a novel heat insulating material, comprising the following steps:
[0051] a. Mix the modified montmorillonite, inorganic fiber, silica and portland cement, introduce into the high mixer, and stir and disperse for 40min at the speed of 1000r / min to obtain the base material;
[0052] b. Add nano-dispersion liquid to the base material, heat at 120°C and stir for 45 minutes, then add absolute ethanol, cool down to 65°C, heat and stir for 15 minutes to obtain material 1;
[0053]c. Add silicon nitride powder, sodium dodecylbenzenesulfonate and activated carbon emulsion to material 1, stir for 30 minutes at a speed of 300r / min, then add binder and opacifier, and stir to obtain a slurry;
[0054] d. Introduce the slurry into the mold, then place it in a vacuum drying oven, dry it at 80°C and a pressure of 5MPa for 4 hours, and then take it out for curing treatment to obtain the finished product.
[0055] The preparation method of the modified montmoril...
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