Preparation method of conductive composite glass fiber yarn

A glass fiber yarn and glass fiber technology, which is applied in the field of preparation of conductive composite glass fiber yarn, can solve the problems of restricting the development of conductive glass fiber, expensive heavy metals, environmental pollution, etc., achieve ideal flexural strength, increase hydroxyl content, The effect of simple and easy preparation process

Inactive Publication Date: 2018-09-21
天长市天意玻璃制品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Electroless plating is one of the common techniques for preparing conductive glass fibers. However, during the plating process, the glass fiber matrix needs to be roughened and activated. These problems have greatly limited the development of electroless plating to prepare conductive glass fibers.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0021] A preparation method of conductive composite glass fiber yarn, comprising the following steps:

[0022] (1) Mix pyrophyllite, kaolin, quartz sand, Glauber's salt, borax, and dolomite in a mass ratio of 60:10:14:3:8:5, put them into a pulverizer, and then send the mixture into a furnace to heat up to 1450°C, keep for 10 hours, and melt to obtain molten glass for later use;

[0023] (2) At 1300°C, the molten glass is cooled and drawn into monofilaments through the bushing plate, and the obtained monofilaments are cooled by water, and then sent to a baking furnace, baked at 350°C for 18 hours, and then taken out and naturally lowered to room temperature spare;

[0024] (3) Put the glass fiber yarn obtained in step (2) into acetone and soak for 50 minutes, take it out and then soak it in 3mol / L hydrochloric acid solution for 80 minutes, wash it with clean water and dry it after completion, and get pretreated glass fiber spare;

[0025] (4) Graphite oxide, N,N-dimethylfor...

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PUM

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Abstract

The invention discloses a preparation method of a conductive composite glass fiber yarn. The conductive composite glass fiber yarn is prepared by pyrophyllite, kaolin, quartz sand, mirabilite, borax,dolomite, graphite oxide, N,N-dimethylformamide, hydriodic acid, acetic acid, calcium hydroxide, ferrous sulfate, hydroxypropyl methyl celluloses and other raw materials. The preparation method disclosed by the invention has the benefits that the glass fiber yarn is prepared by melting and wire-drawing the pyrophyllite, the kaolin, the quartz sand and the other raw materials; the negatively-charged graphite oxide coats the glass fiber surface under the action of electrostatic adsorption; subsequently, the graphite oxide coating the glass fiber surface is reduced by adopting the hydroiodic acidto obtain a graphite-coated glass fiber composite conductive material; finally, the obtained glass fiber yarn has excellent compressive strength, flexural strength and ideal electrical conductivity and has a wide application prospect as a conductive fabric resistant to electromagnetic radiation; meanwhile, the preparation process is simple and easy to implement, the raw materials are cheap and easy to obtain, and the demands of people on the functionality of the glass fiber yarn are met.

Description

technical field [0001] The invention relates to the technical field of glass fiber materials, in particular to a preparation method of conductive composite glass fiber yarn. Background technique [0002] With the advancement of technology, the use of electronic products is expanding by leaps and bounds, and the resulting electromagnetic wave interference has brought many negative effects on the normal operation of electronic equipment and human physiological health. Therefore, electromagnetic shielding materials are becoming more and more popular among people. s concern. In recent decades, the focus of research has shifted more to conductive fibers. The antistatic effect of conductive fibers is more significant and durable, and it is not affected by environmental humidity. When the conductive layer reaches a certain thickness or the conductive component reaches a certain proportion, it has excellent performance. Electromagnetic shielding function, so the development and app...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C13/06C03C25/44C03C25/66D06M11/44D06M11/56D06M15/09
CPCC03C13/06C03C25/44C03C25/66D06M11/44D06M11/56D06M15/09
Inventor 朱炳霞倪敏鹤
Owner 天长市天意玻璃制品有限公司
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