Preparation method of epoxy resin composite material with electric tree resistance characteristic
A technology of epoxy resin and composite materials, which is applied in the field of high-voltage insulating materials, can solve problems that threaten the safe and stable operation of cable transmission systems, partial discharge charges, and electric field concentration, so as to enhance the ability to inhibit the growth of electric branches, promote bonding, and improve The effect of binding density
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[0018] A kind of preparation method of the epoxy resin composite material of electric tree resistance characteristic, comprises the following steps:
[0019] (1) Put micron alumina and nano alumina into acetone solvent at a mass ratio of 1:1.2, ultrasonically disperse for 35 minutes, and wait for use; the average particle size of the micron alumina is 5-10 μm, and the average particle size of the nano alumina is The particle size is 10-20nm;
[0020] Add a certain amount of KH-550 silane coupling agent into the water-acetone solution, adjust the pH value to 5.0 with hydrochloric acid, perform hydrolysis, then add alumina dispersion, stir in a constant temperature water bath at 60°C for 40 minutes, filter under reduced pressure, and use Wash with deionized water until there is no chloride ion, and activate the product at 150°C for 8 hours after drying;
[0021] (2) Low temperature plasma treatment:
[0022] Put the activated and modified alumina powder in the discharge area o...
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