Heat-resistant and salt-resistant high temperature and high pressure filtrate loss reducer for drilling fluid, and preparation method of filtrate loss reducer
A filtrate reducer, high temperature and high pressure technology, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of uncommon fluid loss agents, etc., and achieve good filter loss effect, good filter loss effect, good quality effect
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Embodiment 1
[0023] (1) Weigh 10.34g of acrylic acid, 3.45g of 2-acrylamido-2-methylpropanesulfonic acid, 31.02g of acrylamide, 3.45g of vinylpyrrolidone and 1.72g of nano silicon in a three-necked flask;
[0024] (2) Add a certain amount of distilled water to dissolve the monomer, stir evenly, adjust the pH to 8 with a metered sodium hydroxide aqueous solution, add distilled water to adjust the mass percentage concentration of the system to 60%, and obtain a mixed solution;
[0025] (3) At 50°C, add 0.2 g of each of the initiator ammonium persulfate and sodium bisulfite to the mixed solution, and react and polymerize for 4 hours to obtain a gelatinous block product;
[0026] (4) Crushing and pulverizing the rubber block product to obtain the product fluid loss control agent.
Embodiment 2
[0028] (1) Weigh 5g of acrylic acid, 7.5g of 2-acrylamido-2-methylpropanesulfonic acid, 30g of acrylamide, 5g of vinylpyrrolidone and 2.5g of nano silicon in a three-necked flask;
[0029] (2) Add a certain amount of distilled water to dissolve the monomer, stir evenly, adjust the pH to 9 with a metered sodium hydroxide aqueous solution, add distilled water to adjust the system mass percentage concentration to 60%, and obtain a mixed solution;
[0030] (3) At 60° C., add 0.1 g of the initiator potassium persulfate and sodium bisulfite to the mixed solution, and react and polymerize for 6 hours to obtain a gelatinous block product;
[0031] (4) Crushing and pulverizing the rubber block product to obtain the product fluid loss control agent.
Embodiment 3
[0033] (1) Weigh 14.29g of acrylic acid, 5.71g of 2-acrylamido-2-methylpropanesulfonic acid, 22.86g of acrylamide, 5.71g of vinylpyrrolidone and 1.43g of nano silicon in a three-necked flask;
[0034] (2) Add a certain amount of distilled water to dissolve the monomer, stir evenly, adjust the pH to 8 with a metered sodium hydroxide aqueous solution, add distilled water to adjust the mass percentage concentration of the system to 65%, and obtain a mixed solution;
[0035] (3) At 70°C, add 0.15 g each of the initiator ammonium persulfate and sodium metabisulfite to the mixed solution, and react and polymerize for 5 hours to obtain a gelatinous block product;
[0036] (4) Crushing and pulverizing the rubber block product to obtain the product fluid loss control agent.
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