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34results about How to "Temperature resistance" patented technology

Hydrophobically associating polymer and mixed surfactant binary compound oil displacement system

The invention relates to a hydrophobically associating polymer and mixed surfactant binary compound oil displacement system for use in tertiary oil extraction. The system mainly comprises the following components in percentage by weight: 0.1 to 0.3 percent of hydrophobically associating polymer, 0.1 to 0.6 percent of surfactant and 99.2 to 99.8 percent of water. The hydrophobically associating polymer in the system has high temperature resistance, high salt resistance and viscosity increasing capacity and can largely reduce dosage of polymer; and with high solubilizing capacity, the polymer can increase the dissolution of the surfactant in sewage, thereby increasing the use concentration of the surfactant. The oil displacement system which is dissolved by sewage from extraction can save lots of fresh water; with high viscosity increasing capacity, the system can effectively control flow rate, increase swept volume, increase oil water interface tension to 10<-3>mN / m and increase the oil extraction rate; and because of high stability and injection property, the system can be injected in large dose. According to an indoor oil displacement experiment, the binary compound oil displacement system can improve the extraction rate by over 20 percent compared with that of water displacement. The system without alkali avoids serious damage to the oil layer and corrosion and damage to oilpipes and has a great application prospect.
Owner:SOUTHWEST PETROLEUM UNIV

Amphoteric heat-resistant and salt-resistant filtrate reducer for drilling fluid and preparation method

The invention discloses an amphoteric heat-resistant and salt-resistant filtrate reducer for drilling fluid and a preparation method. The amphoteric heat-resistant and salt-resistant filtrate reducer is prepared from, by weight parts, acrylamide, alkenyl sulfoacid or alkenyl sulphonate, acrylic acid, cationic monomers, rigid monomers, sodium hydroxide, potassium hydroxide, dispersant, deionized water, a molecular weight modifier and an initiator. The preparation method includes the steps that acrylamide, acrylic acid, alkenyl sulfoacid or alkenyl sulphonate, the cationic monomers, the rigid monomers and the deionized water are added into a reactor, after the materials are dissolved, the pH value of the solution is adjusted, the dispersant is added, the materials are mixed, then the mixture is transferred into a reaction still, nitrogen is introduced for deoxygenization, the initiator is added for triggering polymerization, and jelly is taken out after the reaction is completed, dried, smashed and sieved. The molecular weight of the filtrate reducer for the drilling fluid is controllable; the filtrate reducer can adapt to complex drilling conditions, and can be used in horizontal wells, high-temperature deep wells and evaporite beds; fewer residual monomers of the filtrate reducer for the drilling fluid are generated; the filtrate reducer and other oil field chemicals are good in compatibility; the preparation method is simple; the cost is low, and popularization is promoted.
Owner:SHANDONG NUOER BIOLOGICAL TECH

High-temperature resistant secondary cross-linked gel profile control agent and preparation method thereof

The invention discloses a high-temperature resistant secondary cross-linked gel profile control agent and a preparation method thereof, and belongs to the technical field of oilfield chemistry. The profile control agent has good gelling property and high plugging strength and can resist high temperature of 150 DEG C, and the gelling strength and the gelling time can be adjusted. The high-temperature resistant secondary cross-linked gel profile control agent is mainly characterized by the secondary composite crosslinking process, that is, a plugging agent reacts with a first crosslinking agent under the ground condition to form flowable gel similar to weak gel so as to reduce filter loss of the plugging agent in oil deposit during the construction process and reduce the risk of blocking a low-permeability oil flow channel by the plugging agent; and a second crosslinking agent has a second crosslinking reaction under the high-temperature condition of an oil layer to form high-strength gel so as to effectively plug a high-permeability steam flowing channel, and accordingly, steam suction is controlled, and the sweep efficiency is improved. Gelling of the high-temperature resistant secondary cross-linked gel profile control agent is characterized in that micromolecules are inserted into organic macromolecular materials HPAM, and micromolecules and macromolecules mutually permeate, so that a gel system easily performs sizing; and meanwhile, temperature resistance, salt resistance, shear resistance and ageing resistance are enhanced, and the system performance can be well played.
Owner:CHINA PETROLEUM & CHEM CORP +1

Temperature-resistant and salt-resistant hydrophobic association polymer preparation method

The present invention provides a temperature-resistant and salt-resistant hydrophobic association polymer preparation method, which comprises: (1) sequentially adding deionized water, disodium ethylenediaminetetraacetate, an acrylamide monomer, N,N-dioctylacrylamide, 2-acrylamido-2-methylpropanesulfonic acid, a surfactant, a co-solvent, a chain transfer agent and an inorganic salt to a polymerization kettle, uniformly stirring, and cooling to a temperature of 5-10 DEG C under the action of frozen salt water; (2) introducing high purity nitrogen for 1-2 h, adding a multi-stage composite initiator, carrying out an adiabatic polymerization reaction for 5-7 h, taking out a colloid, and granulating; and (3) adding a hydrolysis agent, carrying out hydrolysis for 2-4 h at a temperature of 90-110 DEG C, and drying for 2-3 h at a temperature of 90-110 DEG C to obtain the temperature-resistant and salt-resistant hydrophobic association polymer. According to the present invention, the prepared temperature-resistant and salt-resistant hydrophobic association polymer has advantages of good tackifying property, good temperature resistance, good salt resistance, good shearing resistance, good long-term stability, and high oil displacement efficiency.
Owner:CHINA PETROLEUM & CHEM CORP +1

Temperature-resistant salt-resistant high-expansion plugging agent for plugging large cracks and preparation method thereof

The invention discloses a temperature-resistant salt-resistant high-expansion plugging agent for plugging large cracks and a preparation method of the plugging agent. The plugging agent system comprises the following components in percentage by mass: 6-10% of a main agent, 0.6-1% of a cross-linking agent, 0.006-0.01% of an initiator, 6-14% of an additive and the balance of water, the preparation method provided by the invention comprises the following steps: adding montmorillonite into water to prepare a montmorillonite dispersion system; adding the main agent, the cross-linking agent and theinitiator into the montmorillonite dispersion system to prepare a main agent solution; putting the main agent solution into a drying oven at 90-120 DEG C to gelatinize for 9-48 hours; the gelatinizingstrength of the plugging agent system can reach the H level, the expansion multiple is 50-80 times, the strength after expansion is good, the water plugging effect is good under the conditions of 140DEG C and 250,000 mineralization degrees, and the plugging agent is suitable for profile control and water plugging operation of plugging large-crack water channeling channels of high-temperature andhigh-salinity oil reservoirs.
Owner:SOUTHWEST PETROLEUM UNIV

Association type high-temperature resistant fracturing fluid suitable for volcanic rock fracture

The invention provides an association type high-temperature resistant fracturing fluid suitable for volcanic rock fracture. The fracturing fluid comprises two parts, namely a base liquid and construction additives. The base liquid comprises following components by weight: 0.5-0.9% of a thickening agent and 0.2-0.3% of a flow promoter, with the balance being water. The construction additives comprise a thickening auxiliary agent and a gel breaker. The thickening auxiliary agent is 0.25-0.45% by weight of the base liquid. The gel breaker is 0.02-0.05% by weight of the base liquid. The fracturing fluid belongs to supramolecular structure fluids, and has good viscoelasticity, thus achieving viscoelastic sand carrying. The fracturing fluid has characteristics of capability of being clean and free of residue, good temperature resistance, shearing resistance, shearing dilutability, and the like. During fracturing construction, the fracturing liquid can reduce friction so as to reduce the construction pressure, and the fracturing liquid is low in harm to a reservoir stratum, thus increasing the success rate of fracturing construction, improving fracturing effects, and increasing the productivity of the reservoir stratum. The fracturing liquid is suitable for fracturing transformation of a volcanic rock reservoir stratum.
Owner:CHINA PETROLEUM & CHEM CORP +2

High temperature resistant organic phosphonic acid polymer fluid loss agent, and preparation method and applications thereof

PendingCN109851710AStrong temperature resistanceStrong anti-calcium abilityDrilling compositionMethacrylamideTemperature resistance
The invention provides a high temperature resistant organic phosphonic acid polymer fluid loss agent, and a preparation method and applications thereof. The preparation method comprises following steps: isopropenyl phosphonic acid monomer, an acrylamide monomer, and a sulfonic acid group-containing monomer are subjected to polymerization under the effect of an initiator so as to obtain the high temperature resistant organic phosphonic acid polymer fluid loss agent; wherein the acrylamide monomer is selected from acrylamide, 2-methacrylamide, N-methacrylamide, N-ethyl acrylamide, or N, N-dimethylacrylamide, the sulfonic acid group-containing monomer is selected from 2-acrylamido-2-methylpropane sulfonic acid, p-vinylbenzenesulphonic acid, or alkyl sulfonate. The high temperature resistant organic phosphonic acid polymer fluid loss agent comprises a first repeat unit with a structure represented by formula 1, a second repeat unit with a structure represented by formula 2, and a third repeat unit with a structure represented by formula 3, can be used for preparing drilling fluid which possesses better temperature resistance and salt resistant, and is suitable for high temperature highsalinity drilling fluid systems.
Owner:SINOPEC SSC +1

Acid-resistant and temperature-resistant emulsion type acrylic acid pressure-sensitive adhesive and preparation process thereof

ActiveCN111718675AAlso acid resistantBoth temperature resistanceMacromolecular adhesive additivesEster polymer adhesivesPolymer scienceAdhesive
An acid-resistant and temperature-resistant emulsion type acrylic acid pressure-sensitive adhesive relates to resin packaging, sealing and fixing in the fields of optical lenses, optical materials, electronic information industry and other materials, and comprises a monomer, an emulsifier, an initiator, a residual monomer treating agent, an acid-base number neutralizer, a curing agent and deionized water. According to the technical scheme, a pressure-sensitive adhesion structural mechanics principle is used as a core, lauryl acrylate (LA) and 2-ethylhexyl acrylate (2-EHA) sequence combinationinteraction is emphasized to adjust the acid resistance to be greater than 80 DEG C / 4 hours, and a performance index that the temperature resistance is greater than 120 DEG C / 1 hour is also constructed. The embodiment of the invention discloses an acid-resistant and temperature-resistant emulsion type acrylic acid pressure-sensitive adhesive, which is an oil-to-water benzene-free, halogen-free andformaldehyde-free water-based product, not only solves the problem that a normalized product is restricted by solvent type pressure-sensitive adhesives and harms of organic solvents, but also breaksthrough the technical barriers of acid resistance and temperature resistance accumulated by emulsion type acrylic pressure-sensitive adhesives, and is beneficial to coating, processing and using in the fields of materials such as optical lenses, optical materials and electronic information industries.
Owner:绿色轻化科技发展(北京)有限公司

High temperature resistant organic zirconium crosslinking agent and preparation method thereof, a fracturing fluid jelly and preparation method thereof

The invention discloses a high temperature resistant organic zirconium crosslinking agent and a preparation method thereof. The crosslinking agent is prepared from an inorganic zirconium salt 5%-10%, a polyhydric alcohol 5%-15%, sodium hydroxide 10%-20%, an organic ligand 5%-10%, a complex crosslinking agent 1%-5%, and a heat temperature stabilizer 1%-5% in a water solution. The invention also discloses a fracturing fluid gel prepared from the high temperature resistant organic zirconium crosslinking agent and its preparation method. The fracturing fluid gel is prepared from the high temperature resistant organic zirconium crosslinking agent 0.15%-0.45%, a polyacrylamide thickener 0.3%-0.6%, potassium chloride 0.5%-1%, a temperature stabilizer 0.1%-0.3%, a cleanup additive 0.8%-1.5% and an anti-swelling agent 1.5%-2% with water as a solvent. The high temperature resistant organic zirconium crosslinking agent is suitable for fracturing transformation of an oil reservoir with main characteristics of deep layer, high temperature and low permeability, not only can obviously improve temperature resistance and shearing resistance of a fracturing fluid gel system, but also has a crosslinking delaying performance. And the fracturing fluid gel formed by crosslinking at a temperature of 180-200 DEG C with the polyacrylamide is stable in gel performances, good in temperature resistance and shear resistance, good in hydraulic fracturing effect, and can meet fracturing operation requirements.
Owner:BC P INC CHINA NAT PETROLEUM CORP +1

Raw solution of fracturing fluid, acidified fracturing fluid, water-resistance-reducing and sand-carrying fracturing fluid and its preparation method

The present invention relates to the field of fracturing fluid for oil and gas field reconstruction, in particular to a fracturing fluid stock solution and its preparation method, acidified fracturing fluid, resistance-reducing water and sand-carrying fracturing fluid, wherein the fracturing fluid emulsion is formed by emulsion polymerization, and the The emulsion is formed by mixing the water phase and the oil phase; the acidified fracturing fluid consists of 1.0-2.0% of the emulsion, 1-1.5% of the corrosion inhibitor, 0.5-1% of the iron ion stabilizer, 0.1-0.3% of the acid drainage aid, Made of 10-30% acid and the balance of water, the emulsion is the fracturing fluid stock solution; the resistance-reducing water is composed of 0.04-0.12% of the emulsion, 0.1-0.2% of the drainage aid, 0.2-0.5% of the anti-swelling agent and the balance The sand-carrying fracturing fluid is made of emulsion 1-2.5%, anti-swelling agent 0.2-0.5%, drainage aid 0.15-0.4% and the balance of water. The fracturing fluid stock solution, acidified fracturing fluid, anti-resistance water or suspended sand fracturing fluid of the present invention require different fracturing fluid emulsions, and the on-site construction can adjust the formula at any time according to the actual situation. Good demulsification performance, simple production process, low cost, outstanding temperature resistance and salt resistance.
Owner:FRACTURING COMPANY OF CNPC GREATWALL DRILLING +1

Hydrophobically associating polymer and mixed surfactant binary compound oil displacement system

The invention relates to a hydrophobically associating polymer and mixed surfactant binary compound oil displacement system for use in tertiary oil extraction. The system mainly comprises the following components in percentage by weight: 0.1 to 0.3 percent of hydrophobically associating polymer, 0.1 to 0.6 percent of surfactant and 99.2 to 99.8 percent of water. The hydrophobically associating polymer in the system has high temperature resistance, high salt resistance and viscosity increasing capacity and can largely reduce dosage of polymer; and with high solubilizing capacity, the polymer can increase the dissolution of the surfactant in sewage, thereby increasing the use concentration of the surfactant. The oil displacement system which is dissolved by sewage from extraction can save lots of fresh water; with high viscosity increasing capacity, the system can effectively control flow rate, increase swept volume, increase oil water interface tension to 10<-3>mN / m and increase the oil extraction rate; and because of high stability and injection property, the system can be injected in large dose. According to an indoor oil displacement experiment, the binary compound oil displacement system can improve the extraction rate by over 20 percent compared with that of water displacement. The system without alkali avoids serious damage to the oil layer and corrosion and damage to oilpipes and has a great application prospect.
Owner:SOUTHWEST PETROLEUM UNIV

An acid-resistant, temperature-resistant emulsion-type acrylic pressure-sensitive adhesive and its preparation process

ActiveCN111718675BAlso acid resistantBoth temperature resistanceMacromolecular adhesive additivesEster polymer adhesivesPolymer scienceOptic lens
An acid-resistant and temperature-resistant emulsion-type acrylic pressure-sensitive adhesive, which relates to resin encapsulation, sealing and fixing in the fields of optical lenses, optical materials, electronic information industry and other materials, including monomers, emulsifiers, initiators, residual monomer treatment agents, pH neutralizer, curing agent and deionized water. The technical solution applies the principle of pressure-sensitive adhesive structure mechanics as the core, focusing on the interaction of lauryl acrylate (LA) and 2-ethylhexyl acrylate (2-EHA) sequence combination to adjust acid resistance>80℃ / 4h, both temperature resistance >120℃ / 1h performance index construction. The acid-resistant and temperature-resistant emulsion-type acrylic pressure-sensitive adhesive disclosed in the embodiment of the present invention is an "oil-to-water" benzene-free, halogen-free, and aldehyde-free water-based product, which not only solves the problem that normalized products are subject to solvent-based pressure-sensitive adhesives The restricted use of glue and the harm of organic solvents also break through the technical barriers of acid resistance and temperature resistance accumulated by emulsion-type acrylic pressure-sensitive adhesives, which are beneficial to the coating and processing of optical lenses, optical materials, and electronic information industries.
Owner:绿色轻化科技发展(北京)有限公司
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