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Preparation method of YAl1-xMxO3 (M equals Fe, Co and Cu) nano-pigment

A nano-pigment and doped technology, applied in fibrous fillers and other directions, can solve problems such as difficulty in ensuring quality in large-scale production, cumbersome preparation steps, etc., and achieve the effects of good crystal form, simple and controllable process, and large specific surface area.

Active Publication Date: 2018-12-28
NORTH CHINA UNIV OF WATER RESOURCES & ELECTRIC POWER
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the preparation steps are cumbersome, and it is difficult to guarantee the quality in large-scale production

Method used

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  • Preparation method of YAl1-xMxO3 (M equals Fe, Co and Cu) nano-pigment
  • Preparation method of YAl1-xMxO3 (M equals Fe, Co and Cu) nano-pigment
  • Preparation method of YAl1-xMxO3 (M equals Fe, Co and Cu) nano-pigment

Examples

Experimental program
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Effect test

Embodiment 1

[0045] A kind of preparation method of doped nano pigment, doping YAlO with Fe 3 Nanocrystals, prepared with 0.1 mol of YAl 0.5 Fe 0.5 o 3 For example, include the following steps:

[0046] 1) At room temperature, take 100ml of deionized water and stir it on a magnetic stirrer. Dissolve 12.09 grams of ferric nitrate, 18.76 grams of aluminum nitrate, and 38.31 grams of yttrium nitrate in deionized water in turn. After the above raw materials are completely dissolved, add 0.6g of succinic acid is used as a stabilizer to obtain solution A;

[0047] 2) After the substances in the mixed solution A are completely dissolved, adjust the pH value of the solution A to 6 by dropping ammonia water to obtain the solution B, and then add 1,2 - Propylene Glycol; Obtain mixed solution;

[0048] 3) Stir the mixed solution obtained in step 2) on a constant temperature magnetic stirrer at 60°C for 2h until the solution turns into a gel, then dry, grind, and calcinate at 600°C for 4h to obta...

Embodiment 2

[0050] A kind of preparation method of doped nano pigment, doping YAlO with Fe 3 Nanocrystals, prepared with 0.1 mol of YAl 0.5 Fe 0.5 o 3 For example, include the following steps:

[0051] 1) At room temperature, take 100ml of deionized water and stir it on a magnetic stirrer. Dissolve 12.09 grams of ferric nitrate, 18.76 grams of aluminum nitrate, and 38.31 grams of yttrium nitrate in deionized water in turn. After the above raw materials are completely dissolved, add 0.6g succinic acid is used as a stabilizer to obtain solution A;

[0052] 2) After the substances in the mixed solution A are completely dissolved, adjust the pH value of the solution A to 8 by dropping ammonia water to obtain the solution B, and then add 1,2 -Propylene Glycol, obtain mixed solution;

[0053] 3) Stir the mixed solution obtained in step 2) on a constant temperature magnetic stirrer at 60°C for 2h until the solution turns into a gel, then dry, grind, and calcinate at 600°C for 4h to obtain s...

Embodiment 3

[0055] A kind of preparation method of doped nano pigment, doping YAlO with Fe 3 Nanocrystals, prepared with 0.1 mol of YAl 0.5 Fe 0.5 o 3 For example, include the following steps:

[0056] 1) At room temperature, take 100ml of deionized water and stir it on a magnetic stirrer. Dissolve 12.09 grams of ferric nitrate, 18.76 grams of aluminum nitrate, and 38.31 grams of yttrium nitrate in deionized water in turn. After the above raw materials are completely dissolved, add 0.6g succinic acid is used as a stabilizer to obtain solution A;

[0057] 2) After the substances in the mixed solution A are completely dissolved, adjust the pH value of the solution A to 10 by dropping ammonia water to obtain the solution B, and then add 1,2 -Propylene Glycol, obtain mixed solution;

[0058] 3) Stir the mixed solution obtained in step 2) on a constant temperature magnetic stirrer at 60°C for 2h until the solution turns into a gel, then dry, grind, and calcinate at 600°C for 4 hours to ob...

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Abstract

The invention discloses a preparation method of a YAl1-xMxO3 (M equals Fe, Co and Cu) nano-pigment. The preparation method comprises the following steps: firstly, at normal temperature, taking deionized water, stirring on a magnetic stirrer, sequentially and completely dissolving moderate ferric nitrate, aluminum nitrate and yttrium nitrate into the deionized water according to the molar ratio ofY to Al to Fe, and adding succinic acid as a stabilizer to obtain a solution A after the raw materials are completely dissolved; secondly, after a substance in the mixed solution A is completely dissolved, dropwise adding ammonium hydroxide and adjusting a pH value of the solution A to obtain a solution B, and then adding 1,2-propylene glycol into the solution B to obtain a mixed solution; and thirdly, stirring the mixed solution in the second step on a 60 DEG C thermostatic magnetic stirrer for 2 hours until the solution forms gel, and then drying, grinding and calcining to obtain solid powder. The preparation method disclosed by the invention is green and pollution-free; an obtained product has the advantages of high dispersity, low energy consumption, uniform particles, excellent environment friendliness, low synthetic temperature, simple and controllable process, suitability for large-scale production and the like.

Description

technical field [0001] The invention belongs to the technical field of nano pigments, in particular to a nano pigment YAl with high near-infrared reflection and good durability 1-x m x o 3 (M=Fe, Co, Cu) preparation method. Background technique [0002] Nanoscale inorganic white pigments inherently have a high refractive index (n=2.2 to 2.7) and contribute to light scattering at all wavelengths. They are characterized by high solar absorption in the near infrared region (780 to 2500nm) and ultraviolet (UV) region (290 to 400nm), making them ideal for multifunctional, optically clear surface coatings. Since infrared radiation in the wavelength range of 810 to 1100 nanometers is said to be the main cause of heat, NIR reflective white pigments have become necessary for the design of heat-controlling surface coatings and functional coatings. Furthermore, it has been recognized that the gradual increase in atmospheric temperature is a net effect of CO2 emissions from differen...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09C1/40
CPCC09C1/407
Inventor 仝玉萍张亚辉邢毅王永志陈渊召梅婉婉李克亮张海龙陈希杨中正张瑞珠
Owner NORTH CHINA UNIV OF WATER RESOURCES & ELECTRIC POWER
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