cmp slurry composition for polishing copper and polishing method using same
A composition and slurry technology, applied in polishing compositions containing abrasives, chemical instruments and methods, other chemical processes, etc., can solve the problems of complex manufacturing process, increase in miniaturization, and decrease in yield, etc. The effect of minimizing sag
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[0069] Next, the configuration and effects of the present invention will be described in more detail with reference to some examples. It should be understood that these examples are provided for illustrative purposes only and are not to be construed as limiting the invention in any way.
[0070] Descriptions of details apparent to those skilled in the art will be omitted for clarity.
preparation Embodiment 1
[0072] The water of 20g is placed in the RBF reactor of 100mL, in the reactor, add the acrylic acid (AA) of 2.2g, the methacrylamido tetrazole (MATz) of 0.522g and the initiator (V-50 of 0.64g; 2,2'-Azobis(2-methylpropionamidine) dihydrochloride), then KOH was added to adjust the pH to 12. While refluxing for 30 minutes under a nitrogen atmosphere, the internal temperature of the reactor was raised to 80° C., followed by stirring / heating to perform polymerization for 2 hours, thereby preparing a copolymer I. The molecular weight of Copolymer I was measured by water-soluble GPC and is shown in Table 1. GPC measurement was performed using a Shodex SB806MHQ column with PEO (polyethylene oxide) as a standard. In addition, the molar ratios of acrylic acid (AA) and methacrylamidotetrazole (MATz) in Copolymer I were measured and shown in Table 1.
preparation Embodiment 2
[0074] Copolymer II was prepared in the same manner as in Preparation Example 1 except that 0.16 g of the initiator was added thereto. The molecular weight of Copolymer II was measured by water-soluble GPC and is shown in Table 1. GPC measurement was performed using a Shodex SB806MHQ column with PEO (polyethylene oxide) as a standard. In addition, the molar ratios of acrylic acid (AA) and methacrylamidotetrazole (MATz) in Copolymer II were measured and shown in Table 1.
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