Composite hemostatic material for external trauma and preparation method thereof
A technology of hemostatic material and porous material, which is used in pharmaceutical formulations, bandages, drug delivery, etc., can solve the problem of inability to achieve rapid hemostasis in acute bleeding, and achieve the effects of easy long-term storage, high safety, and good biocompatibility.
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[0039] Example 1
[0040] A method for preparing a composite hemostatic material for external trauma, including the following steps:
[0041] (1) Mix diatomaceous earth and calcium nitrate solution uniformly, the mass ratio of diatomaceous earth to calcium nitrate is 5:1, dry at room temperature, then dry the obtained material, and roast at 500 degrees Celsius for 12 hours;
[0042] (2) Dissolve chitosan in water, add the porous material treated in step (1), the mass ratio of porous material to chitosan is 20:1, mix well and dry.
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[0043] Example 2
[0044] A method for preparing a composite hemostatic material for external trauma, including the following steps:
[0045] (1) The porous material activated carbon, diatomaceous earth, kaolin, and montmorillonite are mixed uniformly with sodium sulfate, calcium nitrate, and ferric chloride solution in a ratio of 1:1:1:1, and the mass ratio of porous material to inorganic salt is 10 :1. Dry at room temperature, then dry the obtained material, and roast it at 600 degrees Celsius for 5 hours;
[0046] (2) Dissolve the agarose in water, add the porous material treated in step (1), the mass ratio of the porous material to the agarose is 4:1, mix well and dry.
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[0047] Example 3
[0048] A method for preparing a composite hemostatic material for external trauma, including the following steps:
[0049] (1) Dissolve the surfactant (hexadecyltrimethylammonium bromide) in the calcium chloride aqueous solution, add sodium silicate under stirring, continue stirring, and let stand for 24 hours, the reaction temperature is 5-80 degrees Celsius ; The mass ratio of the synthetic components is surfactant: sodium silicate = 5:1, calcium chloride aqueous solution: sodium silicate = 50:1 (mass ratio); the concentration of calcium chloride aqueous solution is 10 mmol / L;
[0050] (2) The material obtained in step (1) is heated at 100°C for 24 hours, and the material is filtered dry; after drying, it is calcined at 700°C for 12 hours to obtain a synthetic porous material.
[0051] (3) Mix the synthetic porous material obtained in step (2) with the sodium dihydrogen phosphate solution uniformly, the mass ratio of the synthetic porous material to sodium dihydro...
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