Dendrobium nobile alkaloid eye patch and preparation method thereof
The technology of Dendrobium chinensis and alkaloids is applied in the directions of drug combination, drug delivery, and pharmaceutical formulation, which can solve the problems of high production process requirements and large investment in production equipment, and achieve the effect of relieving eye swelling.
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Embodiment 1
[0049] Dendrobium nobile alkaloid eye patch of the present embodiment, its raw material ratio is:
[0050] Raw materials: Dendrobium nobile alkaloids (preparation method: Dendrobium nobile coarse powder plus 10 times the volume and volume percentage of 70% ethanol aqueous solution for reflux extraction for 2 hours, so a total of 2 extractions, the combined filtrate is concentrated under reduced pressure until it has no alcohol smell and then used with quality Dissolve 5% hydrochloric acid aqueous solution, filter with suction, extract the acid aqueous solution 3 times with petroleum ether, basify it with concentrated ammonia water to pH 10.0, extract the alkaline aqueous solution twice with chloroform, concentrate, and dry) 5g, Cassia anthraquinone (Preparation method: add 10 times the volume of cassia seed coarse powder and 80% ethanol aqueous solution to reflux extraction for 2 hours, extract 3 times in total, combine the extracts to concentrate under reduced pressure and dry...
Embodiment 2
[0059] Dendrobium nobile alkaloid eye patch of the present embodiment, its raw material ratio is:
[0060] Raw material: Dendrobium nobile alkaloid 5g, cassia seed anthraquinone 2g, chrysanthemum flavonoid 2g, Budisma flavonoid 2g, lingonberry flavonoid 2g, borneol 1g, taurine 1g and vitamin C 1g.
[0061] Prepare according to the following specific methods:
[0062] (1) Weigh each raw material according to the formula ratio, add an appropriate amount of ethanol to dissolve, and mix well to obtain a raw material mixture solution (A).
[0063] (2) The skeleton material solution is made of the raw materials in the following mass percentages. Take carbomer (4%), hydroxypropyl methylcellulose (8%), polyvinyl alcohol (5%) and distilled water (balance) in Fully swell in a water bath at 50°C, add sodium hyaluronate (1%), laurocapram (1.5%), glycerin (5%), sodium lauryl sulfate (1.5%), methylparaben (0.2%) , sonicated to obtain a framework material solution.
[0064] (3) Add the ra...
Embodiment 3
[0068] Dendrobium nobile alkaloid eye patch of the present embodiment, its raw material ratio is:
[0069] Raw material: Dendrobium nobile alkaloid 5g, cassia seed anthraquinone 2g, chrysanthemum flavonoid 2g, Budisma flavonoid 2g, lingonberry flavonoid 2g, borneol 1g, taurine 1g and vitamin C 1g.
[0070] Prepare according to the following specific methods:
[0071] (1) Weigh each raw material according to the formula ratio, add an appropriate amount of ethanol to dissolve, and mix well to obtain a raw material mixture solution (A).
[0072] (2) The skeleton material solution is made of the raw materials in the following mass percentages, take carbomer (6%), hydroxypropyl methylcellulose (6%), polyvinyl alcohol (5%) and add distilled water (remainder) in Fully swell in a water bath at 50°C, add sodium hyaluronate (1%), laurocapram (1.5%), glycerin (5%), sodium lauryl sulfate (1.5%), methylparaben (0.2%) , sonicated to obtain a framework material solution.
[0073] (3) Add ...
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