Adhesive layer-equipped polarization film, and image display device
An image display device and adhesive layer technology, which is applied to polarizing elements, lighting devices, layered products, etc., can solve problems such as deterioration, accelerated polarizers, and inability to sufficiently block ultraviolet rays, so as to reduce processes and solve yield reduction. Effect
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manufacture example 1
[0161] Production example 1 (production of acrylic pressure-sensitive adhesive composition (a-1))
[0162] Compounded in a monomer mixture consisting of 78 parts by weight of 2-ethylhexyl acrylate (2EHA), 18 parts by weight of N-vinyl-2-pyrrolidone (NVP) and 4 parts by weight of 2-hydroxyethyl acrylate (HEA) As a photopolymerization initiator, 0.035 parts by weight of 1-hydroxycyclohexyl phenyl ketone (trade name: Irgacure 184, which has an absorption band in the wavelength range of 200 nm to 370 nm, manufactured by BASF Corporation), 0.035 parts by weight of 2,2-dimethyl Oxygen-1,2-diphenylethan-1-one (trade name: Irgacure651, has an absorption band in the wavelength range of 200nm to 380nm, manufactured by BASF Corporation), and then irradiated with ultraviolet light until the viscosity (measurement condition: BH viscometer , No. 5 rotor, 10 rpm, measurement temperature 30° C.) was about 20 Pa·s, thereby obtaining a prepolymer composition (polymerization rate: 8%) obtained b...
manufacture example 2
[0163] Production example 2 (production of acrylic pressure-sensitive adhesive composition (a-2))
[0164]67 parts by weight of butyl acrylate (BA), 14 parts by weight of cyclohexyl acrylate (CHA), 27 parts by weight of 4-hydroxybutyl acrylate (4HBA), 0.05 parts by weight of 2,2-dimethyl Oxygen-1,2-diphenylethan-1-one (trade name: Irgacure 651, has an absorption band in the wavelength range of 200nm to 380nm, manufactured by BASF Japan Co., Ltd.) and 0.05 parts by weight of 1-hydroxycyclohexylphenyl Methanone (trade name: Irgacure 184, which has an absorption band in the wavelength range of 200nm to 370nm, manufactured by BASF Japan Co., Ltd.) was put into a four-neck flask, and partially photopolymerized by exposing it to ultraviolet rays under a nitrogen atmosphere to obtain A partial polymer (monomer syrup) with a polymerization rate of 10% was obtained. Next, 0.15 parts by weight of dipentaerythritol pentaacrylate and dipentaerythritol hexaacrylate (DPHA), and 0.3 parts b...
manufacture example 3
[0165] Production example 3 (manufacture of image display portion side adhesive layer (B-1))
[0166] Put 95 parts of butyl acrylate, 5 parts of acrylic acid, 0.2 parts of azobisisobutyronitrile as a polymerization initiator, and 233 parts of ethyl acetate into a separable flask equipped with a thermometer, a stirrer, a reflux condenser, and a nitrogen gas introduction tube. , and then nitrogen gas was introduced, and nitrogen replacement was performed for about 1 hour while stirring. Then, the flask was heated to 60° C. and reacted for 7 hours to obtain an acrylic polymer having a weight average molecular weight (Mw) of 1.1 million.
[0167] 0.8 parts by weight of trimethylolpropane toluene diisocyanate (trade name: Coronate L, manufactured by Nippon Polyurethane Industry Co., Ltd. ), 0.1 part of a silane coupling agent (trade name: KBM-403, manufactured by Shin-Etsu Chemical Co., Ltd.), thereby preparing an adhesive composition (solution).
[0168] The resulting adhesive c...
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