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Turnable ethylene-propylene-diene rubber heat insulating layer material and preparation method thereof

A technology of EPDM rubber and thermal insulation layer, which is applied in the field of thermal insulation material products, can solve the problems of uniform mixing of components, human harm of dispersive asbestos, supply disconnection, etc., and achieve uniform mixing and supply source. Guaranteed and environmentally friendly components

Inactive Publication Date: 2019-02-22
西安长峰机电研究所
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The commonly used turning heat insulation layer materials suitable for free-filling end-combustion powder columns in China mainly include 5-Ⅲ. The heat insulation layer is a hard heat insulation material containing asbestos. Problem: D303 is a thermal insulation layer material combined with EPDM rubber and chloropropylene rubber. Due to the source of chloropropylene rubber raw materials, there are often supply disconnection problems

Method used

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  • Turnable ethylene-propylene-diene rubber heat insulating layer material and preparation method thereof
  • Turnable ethylene-propylene-diene rubber heat insulating layer material and preparation method thereof
  • Turnable ethylene-propylene-diene rubber heat insulating layer material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] The matrix components and formulations of the insulation materials used are shown in Table 4.

[0032] Table 4 Components and formula of heat insulation material matrix

[0033] serial number

Matrix components

Proportion (weight)

effect

1

EPDM

100

base rubber

2

Zinc oxide

5

activator

3

stearic acid

0.6

plasticizer, activator

4

boron phenolic resin

20

Ablation-resistant filler, carbon forming agent

5

Silicon carbide nanofiller

70

Ablation-resistant, flame-retardant, hardening filler

6

Aramid fiber

4

Ablation-resistant filler, carbonation agent

7

fumed silica

30

Reinforcing agent

8

Antimony oxide

3

flame retardant

9

Decabromodiphenyl ether

8

flame retardant

10

dicumyl per...

Embodiment 2

[0043] The matrix components and formulations of the insulation materials used are shown in Table 6.

[0044] Table 6 Insulation material matrix components and formulations

[0045] serial number

Matrix components

Proportion (weight)

effect

1

EPDM

100

base rubber

2

Zinc oxide

5

activator

3

stearic acid

0.6

plasticizer, activator

4

boron phenolic resin

22

Ablation-resistant filler, carbon forming agent

5

Silicon carbide nanofiller

75

Ablation-resistant, flame-retardant, hardening filler

6

Aramid fiber

6

Ablation-resistant filler, carbonation agent

7

fumed silica

35

Reinforcing agent

8

Antimony oxide

7

flame retardant

9

Decabromodiphenyl ether

10

flame retardant

10

dicumyl perox...

Embodiment 3

[0055] The matrix components and formulations of the insulation materials used are shown in Table 8.

[0056] Table 8 Insulation material matrix components and formulations

[0057]

[0058]

[0059]The manufacturing method process of the thermal insulation material involved in the present invention is:

[0060] (1) Cutting of EPDM rubber and aramid fiber: Cut EPDM rubber into blocks on the rubber cutting machine as required, and cut aramid fiber on the shredding machine, with a length of 3 to 5mm ;

[0061] (2) Weigh each component: Weigh 100 parts of EPDM rubber, 0.6 parts of stearic acid, 5 parts of zinc oxide, 25 parts of boron phenolic resin, 40 parts of fumed silica, and 80 parts of silicon carbide nanofiller according to the formula. parts, 8 parts of aramid fiber, 10 parts of antimony oxide, 12 parts of decabromodiphenyl ether, 8 parts of dicumyl peroxide and other components.

[0062] (3) Preparation of EPDM rubber: Pass the cut EPDM rubber at least 3 times f...

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Abstract

The invention provides a turnable ethylene-propylene-diene rubber heat insulating layer material which is prepared by weighing the components in parts by weight: 100 parts of ethylene-propylene-dienerubber, 5 parts of zinc oxide, 0.6 part of stearic acid, 20-25 parts of boron phenolic resin, 70-80 parts of silicon carbide nanofiller, 4-8 parts of aramid fibers, 30-40 parts of fumed silica, 3-10 parts of antimony oxide, 8-12 parts of decabromodiphenyl ether and 4-8 parts of dicumyl peroxide; sequentially adding ethylene-propylene-diene rubber, stearic acid, zinc oxide, boron phenolic resin, fumed silica, silicon carbide nanofiller, aramid fibers, antimony oxide, decabromodiphenyl ether and dicumyl peroxide into a mixing mill for mixing, and then, carrying out mill run according to the required thickness. The turnable ethylene-propylene-diene rubber heat insulating layer material not only meets requirements for turnability for the location of a free filling end burning grain, uniform mixing, environment friendliness of components and guaranteed supply sources, but also meets heat resistance and anti-scouring performance.

Description

technical field [0001] The invention relates to a thermal insulation material product, which can be used for internal thermal insulation of solid rocket motors. Background technique [0002] The role of the solid rocket motor insulation layer is mainly to protect the combustion chamber shell from being burned through or reduce its strength after being heated, to protect the combustion chamber shell from the corrosion of the grain, and to buffer the bonding stress between the grain and the shell. The commonly used turning heat insulation layer materials suitable for free-filling end-combustion powder columns in China mainly include 5-Ⅲ. The heat insulation layer is a hard heat insulation material containing asbestos. Question: D303 is a thermal insulation layer material combined with EPDM rubber and chloropropylene rubber. Due to the source of chloropropylene rubber raw materials, there are often supply disconnection problems. Contents of the invention [0003] In order to...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08L23/16C08L77/10C08K13/02C08K3/22C08K5/09C08K3/34C08K3/36C08K5/06C08K5/14
CPCC08K2003/2296C08K2201/011C08L23/16C08L2201/08C08L2205/03C08L77/10C08K13/02C08K3/22C08K5/09C08K3/34C08K3/36C08K3/2279C08K5/06C08K5/14
Inventor 张崇耿张海鹏胡大宁邹敏王纪霞包乐张权李晓奋周一博严伟兴祁本利秦锋
Owner 西安长峰机电研究所
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