Synthesis method and application method of "BYP tracer"
A synthesis method and tracer technology, applied in the field of synthesis of a new type of tracer - "BYP tracer", can solve the problems of high detection difficulty, low analysis sensitivity, many steps, etc., to improve detection accuracy, fluorescence Excellent performance and low cost of use
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0038] Preparation of BYP tracer
[0039] 1) Preparation of LiBiF 4
[0040] Accurately measure 60mL of anhydrous ethylene glycol with a graduated cylinder and place it in a beaker, and accurately weigh 4.018g of BiCl with an analytical balance 3 and 1.038g of LiF solid were dissolved in anhydrous ethylene glycol, mixed uniformly, placed in a reaction kettle, and reacted at 150°C for 24h. After cooling, add 100mL deionized water to it, and after the white precipitate is completely precipitated, vacuum filter to obtain LiBiF 4 powder.
[0041] 2) Preparation of LiBiF 4 :Yb 3+ ,Pr 3+
[0042] [c] Preparation of rare earth solution: accurately measure 60mL of deionized water with a measuring cylinder and place it in a beaker, and accurately weigh 0.192g of YbCl with an analytical balance 3 and 0.004g PrCl 3 The solid was dissolved in deionized water.
[0043] [d] Doping: the LiBiF in step 1) 4The powder is evenly dispersed in the rare earth solution in step 2) [a], mix...
Embodiment 2
[0065] Preparation of BYP tracer
[0066] 1) Preparation of LiBiF 4
[0067] Accurately measure 60mL of anhydrous ethylene glycol with a graduated cylinder and place it in a beaker, and accurately weigh 3.789g of BiCl with an analytical balance 3 and 1.038g of LiF solid were dissolved in anhydrous ethylene glycol, mixed uniformly, placed in a reaction kettle, and reacted at 150°C for 24h. After cooling, add 100mL deionized water to it, and after the white precipitate is completely precipitated, vacuum filter to obtain LiBiF 4 powder.
[0068] 2) Preparation of LiBiF 4 :Yb 3+ ,Pr 3+
[0069] [a] Preparation of rare earth solution: accurately measure 60mL of deionized water with a graduated cylinder and place it in a beaker, and accurately weigh 0.018g of PrCl with an analytical balance 3 and 0.384g YbCl 3 Solid dissolved in deionized water;
[0070] [b] Doping: the LiBiF in step 1) 4 The powder is evenly dispersed in the rare earth solution in step 2) [a], mixed unif...
Embodiment 3
[0091] Preparation of BYP tracer
[0092] 1) Preparation of LiBiF 4
[0093] Accurately measure 60mL of anhydrous ethylene glycol with a graduated cylinder and place it in a beaker, and accurately weigh 3.260g of BiCl with an analytical balance 3and 1.038g of LiF solid were dissolved in anhydrous ethylene glycol, mixed uniformly, placed in a reaction kettle, and reacted at 150°C for 24h. After cooling, add 100mL deionized water to it, and after the white precipitate is completely precipitated, vacuum filter to obtain LiBiF 4 powder.
[0094] 2) Preparation of LiBiF 4 :Yb 3+ ,Pr 3+
[0095] [a] Preparation of rare earth solution: accurately measure 60mL of deionized water with a graduated cylinder and place it in a beaker, and accurately weigh 0.107g of PrCl with an analytical balance 3 and 0.767g YbCl 3 Solid dissolved in deionized water;
[0096] [b] Doping: the LiBiF in step 1) 4 The powder is evenly dispersed in the rare earth solution in step 2) [a], mixed unifo...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com