A production process of high-quality aluminum ingots
A production process and high-quality technology, applied in the field of high-quality aluminum ingot production process, can solve the problem of restricting high-quality, high-purity, and high-efficiency products from being put into the market, product purity is not satisfactory, and affects the quality of electrolytic aluminum liquid, etc. problems, to achieve the effect of low production cost, low pollution and high production efficiency
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Embodiment 1
[0022] 1. raw material selection: select alumina powder as raw material, the particle diameter of described alumina powder is 99um, SiO2 in alumina powder 2 , Fe 2 o 3 , Ga 2 o 3 , ZnO, TiO 2 The impurity content is controlled at 78ppm, 78ppm, 40ppm, 4ppm and 38ppm respectively;
[0023] ② Preparation of electrolyte: Add aluminum fluoride to the cryolite mixture so that the molar ratio of sodium fluoride to aluminum fluoride in the cryolite mixture is 2 to 3:1, and then add the mixture mass 2 to the cryolite mixture % calcium fluoride and 10% lithium fluoride are prepared as electrolyte;
[0024] ③Electrolysis: first put the electrolyte prepared in step ② into the electrolytic cell, the material of the electrolytic cell is high-purity graphite, heat the electrolytic cell to 940°C, and then add alumina powder with 5% of the electrolyte mass into the electrolytic cell to obtain The mixed electrolyte in the molten state, then insert the carbon anode into the electrolytic ce...
Embodiment 2
[0031] 1. raw material selection: select alumina powder as raw material, the particle diameter of described alumina powder is 50um, SiO in alumina powder 2 , Fe 2 o 3 , Ga 2 o 3 , ZnO, TiO 2 The impurity content is controlled at 50ppm, 50ppm, 25ppm, 3ppm and 30ppm respectively;
[0032] ② Preparation of electrolyte: Add aluminum fluoride to the cryolite mixture so that the molar ratio of sodium fluoride to aluminum fluoride in the cryolite mixture is 2.5:1, and then add 10% of the mixture mass to the cryolite mixture Calcium fluoride and 6% lithium fluoride are prepared as electrolyte;
[0033] ③Electrolysis: first put the electrolyte prepared in step ② into the electrolytic cell, the material of the electrolytic cell is high-purity graphite, heat the electrolytic cell to 950°C, and then add alumina powder with an electrolyte mass of 6% to the electrolytic cell to obtain A mixed electrolyte in a molten state, and then insert a carbon anode into the electrolytic cell. The...
Embodiment 3
[0040] 1. raw material selection: select alumina powder as raw material, the particle diameter of described alumina powder is 20um, SiO2 in alumina powder 2 , Fe 2 o 3 , Ga 2 o 3 , ZnO, TiO 2 The impurity content is controlled at 50ppm, 30ppm, 30ppm, 1ppm and 30ppm respectively;
[0041] ② Preparation of electrolyte: Add aluminum fluoride to the cryolite mixture so that the molar ratio of sodium fluoride to aluminum fluoride in the cryolite mixture is 3:1, and then add 15% of the mixture mass to the cryolite mixture Calcium fluoride and 2% lithium fluoride are prepared as electrolyte;
[0042] ③Electrolysis: first put the electrolyte prepared in step ② into the electrolytic cell, the material of the electrolytic cell is high-purity graphite, heat the electrolytic cell to 960°C, and then add alumina powder with 10% of the electrolyte mass into the electrolytic cell to obtain A mixed electrolyte in a molten state, and then insert a carbon anode into the electrolytic cell. ...
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