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Printing ink using inorganic nanometer material and preparation method and application thereof

A technology for inorganic nanomaterials and printing inks, applied in inks, applications, household appliances, etc., can solve the problems of comprehensive stability, dispersion, viscosity, stability, surface tension and volatility of inorganic nanomaterial printing inks. Achieve good hydrophobic stability and dispersion performance, uniform film formation, and ensure the effect of charge transport

Inactive Publication Date: 2019-05-28
SHENZHEN TCL IND RES INST
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0005] The object of the present invention is to provide a kind of inorganic nano material printing ink and preparation method thereof, aim at solving the comprehensive stability (including dispersibility, viscosity, stability, surface tension and volatility) of existing inorganic nano material printing ink is difficult to take into account The problem

Method used

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preparation example Construction

[0117] Correspondingly, an embodiment of the present invention provides a method for preparing an inorganic nanomaterial printing ink, comprising the following steps:

[0118] S01. Provide inorganic nanomaterials and organic solvents, the organic solvents contain at least one fluorine-containing organic solvent;

[0119] S02. Dissolving the inorganic nanomaterials in an organic solvent to form the inorganic nanomaterial printing ink.

[0120] The preparation method of the inorganic nanomaterial printing ink provided in the embodiment of the present invention only needs to dissolve the inorganic nanomaterial in an organic solvent containing a fluorine-containing solvent with a specific structure, the operation is simple and easy to control, and no strict conditions are required. Mass production is possible.

[0121] Specifically, in the above step S01, the type of the fluorine-containing organic solvent can be referred to above, specifically, if the organic solvent contains at...

Embodiment 1

[0134] An inorganic nanomaterial printing ink, comprising oleylamine-stabilized quantum dots, organic solvents and auxiliary reagents, wherein the mass ratio of the oleylamine-stabilized quantum dots to the organic solvent is 10:90; the organic solvent consists of 100% by weight The content is 80% of 1-butylnaphthalene solvent and 20% by weight of dimethoxymethyl (3,3,3-trifluoropropyl) silicon solvent, and 1-butylnaphthalene and The dimethoxymethyl (3,3,3-trifluoropropyl) silicon is refined to a purity greater than 99.9% by removing water and oxygen; the auxiliary reagent is polypyrrole.

[0135] A method for preparing an inorganic nanomaterial thin film, comprising the following steps:

[0136] S11. Weigh each component according to the formula of the above-mentioned inorganic nanomaterial printing ink;

[0137] S12. Provide a 500mL single-necked flask, and add oleylamine-stabilized red CdSe / ZnS quantum dots, 1-butylnaphthalene, polypyrrole and dimethoxymethyl (3,3,3-triflu...

Embodiment 2

[0140] An inorganic nanomaterial printing ink, comprising oleylamine-stabilized quantum dots and an organic solvent, wherein the mass ratio of the oleylamine-stabilized quantum dots to the organic solvent is 8:92; the organic solvent consists of a weight percentage of 55% of 1-(methoxymethoxy)naphthalene, 30% by weight of cyclohexylbenzene and 15% by weight of triethoxy-1H,1H,2H,2H-tridecane Fluoro-N-octylsilane solvent composition, and 1-(methoxymethoxy)naphthalene, cyclohexylbenzene, triethoxy-1H,1H,2H,2H-tridecafluoro-N-octylsilane solvent All have been refined by dehydration and oxygen removal to a purity greater than 99.9%.

[0141] A method for preparing an inorganic nanomaterial thin film, comprising the following steps:

[0142] S21. Weigh each component according to the formula of the above-mentioned inorganic nanomaterial printing ink;

[0143]S22. Provide a 500mL high-density polyethylene bottle, and in the case of stirring, add oleylamine-stabilized green CdZnSe / ...

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Abstract

The invention provides a printing ink using an inorganic nanometer material. The printing ink using the inorganic nanometer material adopts an organic solvent, and comprises at least one type of inorganic nanometer material and at least one type of fluorine-containing alcohol organic solvent, wherein the structure of the fluorine-containing alcohol organic solvent is shown in a structural formulaVIII, namely [(Rb')n'-(Rfb)n-(Rfa)m-(Ra')m']-OH; in the formula VIII, Rfa and Rfb are independently selected from partially or totally fluorated alkyl and aryl; Ra' and Rb' are independently selectedfrom H (hydrogen), fatty group with C1 to C30, aromatic group, F (fluorine), Cl (chloride), Br (bromine) and I (iodine); -OH is connected with carbon atom, and is not directly connected with benzene ring carbon; the value ranges of m, n, m', and n' meet the requirements that m and n are respectively 0 or 1, and m and n are not simultaneously 0; m' and n' are respectively 0 or 1.

Description

technical field [0001] The invention belongs to the technical field of electroluminescent diode display, and in particular relates to an inorganic nanometer material printing ink and a preparation method thereof. Background technique [0002] Quantum dot (QD), also known as nanocrystal, is a nanoparticle composed of II-VI or III-V elements. Quantum dots are zero-dimensional (zero-dimensional) nano-semiconductor materials, and the size of the three dimensions is not larger than twice the exciton Bohr radius of the corresponding semiconductor material. The performance of quantum dots is generally affected by the quantum confinement effect ( quantum confinement effect), surface effects and doping effects. The particle size of quantum dots is generally between 1 and 10 nm. Since electrons and holes are quantum-confined, the continuous energy band structure becomes a discrete energy level structure with molecular characteristics, and can emit fluorescence after being excited. Q...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D11/36C09D11/38C09D11/30
Inventor 李雪
Owner SHENZHEN TCL IND RES INST
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