Textile finishing agent preparation method

A technology of fabric finishing agent and auxiliary agent, applied in the field of fabric finishing agent preparation, can solve the problems of poor fabric bonding performance, poor effect of fabric finishing agent, easy loss of titanium dioxide, etc. The effect of bonding

Inactive Publication Date: 2019-07-09
常州琨瑶纺织品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The technical problem to be solved by the present invention: aiming at the problem that the titanium dioxide in the current fabric finishing agent is easy to lose and has

Method used

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  • Textile finishing agent preparation method

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0025] The preparation method of the conditioning liquid is to mix silk fibroin, maleic anhydride and glacial acetic acid in a mass ratio of 3:1:9-12 to obtain the conditioning liquid.

[0026] The auxiliary agent is aminopropyltriethoxysilane.

[0027] The additives are mixed with thiosemicarbazide and hydroxyethyl methacrylate in a mass ratio of 9:1 to 2.

[0028] The preparation method of the additive liquid is as follows: the surface active agent, the metal salt, and the mixed solvent are mixed in a mass ratio of 1:6 to 8:16 to obtain the additive liquid.

[0029] The surfactant is any one of isotridecyl alcohol polyoxyethylene ether and sodium dodecylbenzene sulfonate.

[0030] The metal salt is a mixture of platinum nitrate and zinc nitrate in a mass ratio of 4:1 to 6.

[0031] The mixed solvent is a mixture of salicylic acid solution and ethanol solution in a volume ratio of 3:6-8.

[0032] The auxiliary solvent is a mixture of tetrahydrofuran and petroleum ether in a volume ratio ...

Example Embodiment

[0040] Example 1

[0041] The preparation method of the conditioning liquid is to mix silk fibroin, maleic anhydride and glacial acetic acid in a mass ratio of 3:1:12 to obtain the conditioning liquid.

[0042] The auxiliary agent is aminopropyltriethoxysilane.

[0043] The additives are thiosemicarbazide and hydroxyethyl methacrylate mixed in a mass ratio of 9:2.

[0044] The preparation method of the additive liquid is as follows: the surfactant, the metal salt, and the mixed solvent are mixed in a mass ratio of 1:8:16 to obtain the additive liquid.

[0045] The surfactant is sodium dodecylbenzene sulfonate.

[0046] The metal salt is a mixture of platinum nitrate and zinc nitrate in a mass ratio of 4:6.

[0047] The mixed solvent is a mixture of salicylic acid solution and ethanol solution in a volume ratio of 3:8.

[0048] The auxiliary solvent is a mixture of tetrahydrofuran and petroleum ether in a volume ratio of 6:3.

[0049] The auxiliary agent is a mixture of ammonium citrate and ...

Example Embodiment

[0056] Example 2

[0057] The preparation method of the conditioning liquid is to mix silk fibroin, maleic anhydride and glacial acetic acid in a mass ratio of 3:1:11 to obtain the conditioning liquid.

[0058] The auxiliary agent is aminopropyltriethoxysilane.

[0059] The additives are mixed with thiosemicarbazide and hydroxyethyl methacrylate in a mass ratio of 9:1.5.

[0060] The preparation method of the additive liquid is as follows: the surfactant, the metal salt, and the mixed solvent are mixed in a mass ratio of 1:7:16 to obtain the additive liquid.

[0061] The surfactant is isomerized tridecanol polyoxyethylene ether.

[0062] The metal salt is a mixture of platinum nitrate and zinc nitrate in a mass ratio of 4:5.

[0063] The mixed solvent is a mixture of salicylic acid solution and ethanol solution in a volume ratio of 3:7.

[0064] The auxiliary solvent is a mixture of tetrahydrofuran and petroleum ether in a volume ratio of 6:2.

[0065] The auxiliary agent is a mixture of am...

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Abstract

The invention relates to a textile finishing agent preparation method, and belongs to the technical field of textile additives. Silk fibroin, maleic anhydride and tetrabutyl titanate serve as raw materials for preparing titanium dioxide, electrostatic attraction between the titanium dioxide and the silk fibroin is easily formed, imido combined hydrogen ions have positive charge, the surface of thesilk fibroin further contains rich hydroxy groups, the hydroxy groups and amino generated by auxiliary hydrolysis can form hydrogen bonds, and reaction activity is improved. The hydrogen bonds are inhybrid reaction with thiosemicarbazide, hydroxyethyl methylacrylate and the like, and the ultraviolet resistance and the antibacterial performance of a finishing agent are improved. The titanium dioxide is deposited on the surface of the silk fibroin and can be effectively combined with a fabric by the aid of rich active groups in the silk fibroin, the titanium dioxide and the fabric have good fusion properties by the aid of properties of the silk fibroin, the combination degree of the titanium dioxide and the fabric is further increased by an organic ligand formed on the surface of the titanium dioxide, and water resistance is enhanced under the action of aminopropyltriethoxysilane.

Description

Technical field [0001] The invention relates to a preparation method of a fabric finishing agent, belonging to the technical field of textile additives. Background technique [0002] Ultraviolet rays are prone to adverse effects on textiles. After silk is irradiated by ultraviolet, the C-N bond of the peptide bond group in the main chain of the molecular chain and the side group is broken, releasing CO and N 2 Wait for the gas to finally decompose into amino acids. High-performance fibers will also experience varying degrees of performance degradation under ultraviolet radiation. For example, after polyparaphenylene benzodioxazole (PBO) fibers are irradiated with ultraviolet rays, their internal carbon atoms are oxidized to CO and CO 2 And so on, and CO can further accelerate oxidation. At the same time, the hydrogen atoms in the polymer are oxidized to -COOH, and then the bimolecular decomposes to generate free radicals, attack PBO macromolecules, destroy the chemical structure...

Claims

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Application Information

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IPC IPC(8): D06M11/46D06M15/15D06M13/513D06M13/432
CPCD06M11/46D06M13/432D06M13/513D06M15/15D06M16/00D06M2200/25
Inventor 李璐
Owner 常州琨瑶纺织品有限公司
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