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Microencapsulation method capable of increasing stability of anthocyanin, product prepared by microencapsulation method and use of product

A technology of microencapsulation and glycoside stability, which is applied in the field of pigment preparation, can solve problems such as poor stability, and achieve the effects of increasing stability, ensuring stability, and simple process

Inactive Publication Date: 2019-07-16
WUHAN POLYTECHNIC UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Anthocyanin (Anthocyanin) is a kind of water-soluble natural colorant, which has certain biological activities such as anti-oxidation and anti-inflammation. Therefore, the encapsulation technology is used to improve the stability of anthocyanins and expand the scope of application
[0003] At present, the commonly used methods for microencapsulation of anthocyanins include spray drying, liposome, and coacervation. Among them, spray drying is the most commonly used encapsulation technology in the food industry. During the spray drying process, the solvent evaporates quickly, and the active ingredient is instantly absorbed Retain to form an amorphous solid dispersion. This method has simple process and low cost, and is suitable for active substances sensitive to temperature. The spray drying method has been proved to be effective in protecting polyphenol compounds, but its high temperature conditions are limited May degrade heat-sensitive anthocyanins

Method used

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  • Microencapsulation method capable of increasing stability of anthocyanin, product prepared by microencapsulation method and use of product
  • Microencapsulation method capable of increasing stability of anthocyanin, product prepared by microencapsulation method and use of product
  • Microencapsulation method capable of increasing stability of anthocyanin, product prepared by microencapsulation method and use of product

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Effect test

Embodiment 1

[0055] In the present embodiment, the microencapsulation method for improving the stability of anthocyanins comprises the following steps:

[0056] S1. Using sodium alginate as the wall material, prepare 2 g of sodium alginate, 1 g of calcium carbonate and 15 mL of water (in this embodiment) respectively according to the weight ratio of sodium alginate: calcium carbonate: water = 2:1:15. , the weight of every mL of water is regarded as 1g, and the above-mentioned weight units and volume units are correspondingly expanded by the same multiple and also belong to the scope of protection of the present embodiment), then the sodium alginate and calcium carbonate are added to the water to swell for 1h, with Obtain wall material gel system;

[0057] S2. Dissolve 1 mg of lyophilized anthocyanin in distilled water to prepare a 1 mg / mL anthocyanin solution, using anthocyanin as the core material, fully mix the wall material gel system with 166.7 mL of anthocyanin solution for use , and...

Embodiment 2

[0072] In the present embodiment, the microencapsulation method for improving the stability of anthocyanins comprises the following steps:

[0073] S1. Using sodium alginate as the wall material, prepare 3 g of sodium alginate, 1 g of calcium carbonate and 20 mL of water respectively according to the weight ratio of sodium alginate: calcium carbonate: water = 3:1:20, and then mix the Sodium alginate and calcium carbonate are added to the water to swell for 2 hours to obtain a wall material gel system;

[0074] S2. Dissolving 1 mg of lyophilized anthocyanin in distilled water to prepare a 1 mg / mL anthocyanin solution, using anthocyanin as the core material, fully mixing the wall material gel system with 200 mL of anthocyanin solution for use, And make according to the weight ratio, sodium alginate: anthocyanin = 15: 1, to obtain the water phase;

[0075] S3. In terms of volume ratio, take Span80 and vegetable oil according to Span80:vegetable oil=2:1, and mix the Span80 and ve...

Embodiment 3

[0089] S1. Using sodium alginate as the wall material, prepare the sodium alginate 4g, calcium carbonate 1g and water 25mL respectively according to the weight ratio of sodium alginate: calcium carbonate: water = 4:1:25, and then mix the Sodium alginate and calcium carbonate are added to the water to swell for 2 hours to obtain a wall material gel system;

[0090] S2. Dissolving 1 mg of lyophilized anthocyanin in distilled water to prepare a 1 mg / mL anthocyanin solution, using anthocyanin as the core material, fully mixing the wall material gel system with 200 mL of anthocyanin solution for use, And make according to the weight ratio, sodium alginate: anthocyanin = 20: 1, to obtain the water phase;

[0091] S3. In terms of volume ratio, take Span80 and vegetable oil according to Span80:vegetable oil=1.5:1, and mix the Span80 and vegetable oil to obtain an oil phase, and the vegetable oil is preferably soybean oil; and in volume ratio, according to Water phase: oil phase = 4:1...

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Abstract

The invention discloses a microencapsulation method capable of increasing stability of anthocyanin, a product prepared by the microencapsulation method and use of the product. The microencapsulation method comprises the following steps of S1, using sodium alginate as a wall material, adding the sodium alginate and calcium carbonate to water, and performing swelling for 1-2h so as to obtain a wallmaterial gel system; S2, using anthocyanin obtained through a special preparation technology as a core material, sufficiently and uniformly mixing the wall material gel system with a anthocyanin solution for standby application so as to obtain a water phase; S3, mixing Span80 with vegetable oil so as to obtain an oil phase, mixing the water phase with the oil phase, performing magnetic stirring, and performing emulsifying so as to obtain W / O emulsion; and S4, adjusting the pH of the W / O emulsion to acid, mixing the W / O emulsion with a table salt buffer solution, performing standing for 1-2h, and separating the oil phase from the water phase so as to obtain liquid anthocyanin microcapsules. The anthocyanin is prepared through a special preparation technology, so that yield and purity are increased; and besides, the microencapsulation method and the drying condition of the anthocyanin are optimized through improved technological parameters, so that the structural stability of the anthocyanin is guaranteed, and the cost is reduced.

Description

technical field [0001] The invention relates to the field of pigment preparation. More specifically, the present invention relates to a microencapsulation method for improving the stability of anthocyanins and its products and uses. Background technique [0002] Anthocyanin (Anthocyanin) is a kind of water-soluble natural colorant, which has certain biological activities such as anti-oxidation and anti-inflammation. Therefore, the encapsulation technology is used to improve the stability of anthocyanins and expand the scope of application. [0003] At present, the commonly used methods for microencapsulation of anthocyanins include spray drying, liposome, and coacervation. Among them, spray drying is the most commonly used encapsulation technology in the food industry. During the spray drying process, the solvent evaporates quickly, and the active ingredient is instantly absorbed Retain to form an amorphous solid dispersion. This method has simple process and low cost, and...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L33/105A23L5/43A23L29/00A23P10/30C07D311/62A61K9/52A61K31/352A61P39/06A61P29/00
CPCA23L33/105A23L5/43A23L29/035A23P10/30C07D311/62A61K9/5036A61K31/352A61P39/06A61P29/00A23V2002/00B01D61/149A23V2200/04A23V2200/30A23V2250/022A23V2250/21A23V2250/5026A23V2300/14A23P10/35B01D15/203B01D15/426A61K9/501A61K9/5015B01D61/58B01D61/027B01D2311/2642B01D61/025B01D2311/2626A23L29/256A23L29/015A61K9/5089A61K47/22B01D61/04B01D61/145B01D61/147B01D61/16B01D69/02B01D2311/04B01D2311/06B01D2311/2649B01D2311/2676
Inventor 何静仁周兰张瑞毛莹杨宁李书艺何毅祝振洲
Owner WUHAN POLYTECHNIC UNIVERSITY
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