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Preparation method of iron-based composite material

A technology of iron-based composite materials and composite powders, which is applied in the field of metal-based composite materials and advanced manufacturing, can solve the problems of waste liquid discharge, poor corrosion resistance, and low surface hardness of ferroalloys, and achieve the effect of simple process and excellent mechanical properties

Active Publication Date: 2019-07-23
SOUTHWEST JIAOTONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] Using Fe-N powder as raw material, by controlling the phase transition behavior of Fe-N during sintering, an iron alloy with micro-nano porous structure with excellent comprehensive mechanical properties was prepared without adding any foaming agent or pore-forming agent (ZL201310046622 .3), but due to the low surface hardness and poor corrosion resistance of this ferroalloy, it is limited in the preparation of gears, bearings and other parts with vibration reduction and damping properties
[0004] Fe-Ni-P alloy is a new type of high-performance alloy with high phosphorus content (ZL201710448064.1) newly developed through powder metallurgy technology in recent years. This alloy has excellent mechanical properties and corrosion resistance, and can replace stainless steel powder metallurgy products It is used in the manufacture of high-end precision parts such as high-precision gears and bearings. However, due to the high preparation cost of Fe-Ni-P composite powder, it will also generate waste liquid discharge, which has a certain impact on the environment and limits its further development and development. application

Method used

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  • Preparation method of iron-based composite material
  • Preparation method of iron-based composite material
  • Preparation method of iron-based composite material

Examples

Experimental program
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Effect test

Embodiment 1

[0026] A kind of preparation method of iron-based composite material, such as image 3 As shown in -a, take 2 parts of Fe-Ni-P composite powder 3 with an average particle diameter of 1 micron, and Ni and P mass percentages of 28% and 1.5%, each with 9 grams; weigh 27 grams of the average Fe—N powder 4 with a particle size of 100 nanometers and a mass percentage of nitrogen of 8% means that the mass proportions of the two powders are 20%*2 and 60% respectively. Put 9 grams of Fe-Ni-P composite powder 3, 27 grams of Fe-N powder 4, and 9 grams of Fe-Ni-P composite powder 3 into a graphite mold 2 with an internal diameter of 2 centimeters and a height of 6 centimeters. The length of the feeding section of the lower pressing head 6 is selected to be 1 cm, and the length of the feeding section of the upper pressing head 1 is 3 cm, and pre-pressing is performed under an axial pressure of 20 MPa to make the powders fully contact. Then use spark plasma sintering (SPS) technology for s...

Embodiment 2

[0028]A preparation method of an iron-based composite material, weighing 2 parts of Fe-Ni-P composite powder 3 with an average particle size of 1.17 microns and a Ni and P mass percent content of 28.33% and 1.57%, respectively, 8.68 grams per part; Weighed 27.9 grams of Fe—N powder 4 with an average particle size of 125 nm and a mass percentage of nitrogen of 8.33%, that is, the mass proportions of the two powders were 19.16%*2 and 61.68%, respectively. Put 8.68 grams of Fe-Ni-P composite powder 3, 27.9 grams of Fe-N powder 4, and 8.68 grams of Fe-Ni-P composite powder 3 into a graphite mold 2 with an inner diameter of 2 cm and a height of 6 cm. The length of the feeding section of the lower pressing head 6 is selected to be 1 cm, and the length of the feeding section of the upper pressing head 1 is 2.83 cm. Pre-pressing is performed under an axial pressure of 20 MPa to make the powders fully contact. Then use spark plasma sintering (SPS) technology to carry out sintering and ...

Embodiment 3

[0030] A preparation method of an iron-based composite material, weighing 2 parts of Fe-Ni-P composite powder 3 with an average particle diameter of 1.34 microns, and Ni and P mass percentages of 28.66% and 1.64%, respectively, 8.2 grams per part; Weighed 28.3 grams of Fe—N powder 4 with an average particle size of 150 nm and a mass percentage of nitrogen of 8.66%, that is, the mass proportions of the two powders were 18.33%*2 and 63.34% respectively. Put 8.2 grams of Fe-Ni-P composite powder 3, 28.3 grams of Fe-N powder 4, and 8.2 grams of Fe-Ni-P composite powder 3 into a graphite mold 2 with an inner diameter of 2 centimeters and a height of 6 centimeters. The length of the feeding section of the lower pressing head 6 is selected to be 1 cm, and the length of the feeding section of the upper pressing head 1 is 2.66 cm. The pre-pressing molding is performed under an axial pressure of 20 MPa to fully contact the powders. Then use spark plasma sintering (SPS) technology to car...

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Abstract

The invention provides a preparation method of an iron-based composite material, and relates to the technical field of metal matrix composite materials and advanced manufacturing. Fe-Ni-P composite powder with the particle size being 1-2 microns and Fe-N powder with the particle size being 100-250 nm are used as raw materials; and the size and the axial displacement of a graphite die pressing headare controlled to achieve control over the porous iron porosity, and the Fe-Ni-P alloy / porous Fe / Fe-Ni-P alloy composite material with the porosity being 14% to 39% is prepared. The weight of the Fe-Ni-P alloy is reduced, and meanwhile, the good shock absorption and damping properties are obtained. On the other hand, subsequent cryogenic treatment of a shaped sample can induce conversion from themetastable state gamma phase in a surface layer Fe-Ni-P alloy to the alpha phase, the hardness strength is remarkably improved accordingly, the phase change degree can be controlled by changing the cryogenic treatment temperature and holding time, and the adjustment of the surface layer properties is further achieved.

Description

technical field [0001] The invention relates to the technical field of metal matrix composite materials and advanced manufacturing. Background technique [0002] High-strength, light-weight, and multi-functional composites have always been the development direction of metal matrix composites. Metal matrix composites with a dense surface and a porous middle with a sandwich structure are a new type of composite material developed in recent years. The dense structure of the surface retains the excellent mechanical properties of traditional metal materials, while the porous structure of the middle layer effectively reduces The density of the material also gives the material vibration and noise reduction and damping properties. The metal matrix composite material with this kind of composite structure has good application value and market prospect in the fields of mechanical engineering, aerospace, automobile, high-speed train and so on. [0003] Using Fe-N powder as raw materia...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F3/105B22F3/11B22F7/02C22C38/08
CPCB22F3/105B22F3/11B22F7/02C22C38/002C22C38/08C22C38/001B22F2003/1051B22F7/06B22F3/1007B22F3/162B22F2301/15B22F2301/35B22F2302/45B22F2304/10
Inventor 崔国栋刘瑜轩张程菘陈宜飞徐沁
Owner SOUTHWEST JIAOTONG UNIV
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