Preparation method of nano titania for air purification
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A nano-titanium dioxide and air purification technology, which is applied in the direction of titanium dioxide, titanium oxide/hydroxide, nanotechnology, etc., can solve the problems of excessive discharge of three wastes, poor product quality, and high technical difficulty, and achieve improved purity, low cost, and improved The effect of quantum effects
Inactive Publication Date: 2019-08-02
广州三木环保科技有限公司
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However, high-grade raw materials are required, and rutile ore is used, which is a scarce resource; the technology is difficult, and materials and equipment that are resistant to titanium tetrachloride, chlorine, and oxygen are required at high temperatures. The investment cost is high, maintenance is difficult, and the advantages are gone.
The sulfuric acid method has cheap raw materials, mature technology, and simple equipment, but the process is long, high energy consumption, high discharge of three wastes, and poor product quality
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[0024] In order to make the purpose, technical solutions and advantages of the present invention clearer, the present invention will be further described in detail below in conjunction with specific embodiments. It should be understood that these descriptions are exemplary only, and are not intended to limit the scope of the invention. Also, in the following description, descriptions of well-known structures and techniques are omitted to avoid unnecessarily obscuring the concept of the present invention.
[0025] A method for preparing air-purifying nano-titanium dioxide proposed by the present invention comprises the following steps:
[0026] S1, select ilmenite ore, and process the ilmenite ore into powder;
[0027] S2, add concentrated hydrochloric acid to powdery ilmenite ore and carry out acidolysis, the ore-acid ratio of dissolving ore is 4-6, and acidolysis temperature is 50-100 degree centigrade; Leave standstill 1-2 hour after acidolysis dissolving ore, then Filter ...
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Abstract
A preparation method of nano titania for air purification comprises steps as follows: titanium iron ore is selected and processed into powder; concentrated sulfuric acid is added to the powdery titanium iron ore for acidolysis; still standing is performed after the ore is dissolved through acidolysis, slag is removed through filtration, and a primary filtered titanium liquid A is obtained; the titanium liquid A is cooled to the normal temperature and crystalized to separate iron dichloride tetrahydrate, and a secondary filtered titanium liquid B is obtained through filtration; an oxidizing agent is added to the secondary filtered titanium liquid B, and a solution D is obtained; cerium nitrate is added to the solution D, sodium hydroxide is added, the PH is adjusted to be alkaline, and sufficient mixing is performed; activated carbon fiber is added, soaking is performed under the ultrasonic condition, and a mixed liquid D is obtained; the mixed liquid D is aired, calcined and ground into powder, and cerium-doped nano titania powder is obtained. The nano titania is small in particle size and good in dispersity, the quantum effect of the nano titania is improved, and the air purification effect is improved; the reaction process is environmentally friendly and pollution-free.
Description
technical field [0001] The invention relates to the field, in particular to a method for preparing air-purifying nano-titanium dioxide. Background technique [0002] Titanium dioxide has stable physical properties, chemical properties, excellent optical and electrical properties, and excellent pigment performance, so it is widely used. Coatings, plastics, rubber, chemical fibers, papermaking, inks, cosmetics, toys, capacitors, picture tubes, cutting-edge defense technology, food, medicine, chemical reagents, welding electrodes, enamel, ceramics, glass, refractory materials, metallurgy, artificial gemstones, art paints Titanium dioxide is used in food, leather, printing and dyeing paste, soap, catalyst, etc. [0003] At present, the production of titanium dioxide mainly includes the chloride method and the sulfuric acid method. The chlorination method has advanced technology, short process, easy automation and good product quality. However, high-grade raw materials are req...
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