Method for efficiently preparing graphene
A graphene and high-efficiency technology, applied in the field of high-efficiency preparation of graphene, can solve the problems of not easy cleaning, long time consumption, and difficult solid-liquid separation, etc., to achieve low raw material cost, strong operability, and good powder fluidity Effect
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Embodiment 1
[0033] Embodiment 1 of the present invention discloses a method for efficiently preparing graphene, and the technical scheme adopted is as follows:
[0034] A method for efficiently preparing graphene, comprising the following steps:
[0035] S1, take 3g of 325 mesh natural flake graphite as raw material and 1.5g of sodium nitrate, add 150ml of concentrated sulfuric acid and stir for 60min, the stirring rate is 300-500rpm, the temperature of the reaction material is controlled at 5°C±1°C, and add to the mixing system in batches 12g potassium permanganate, react for 100min, heat up to 40°C, continue stirring for 2h;
[0036] S2, remove the reaction mixture obtained in step S1 from the water bath, cool to room temperature, stir and slowly add 90ml of pure water to dilute, control the temperature at 90°C for 30min, cool the reaction system naturally, lower the temperature to 50°C, stir and add 200ml at a temperature of 50°C of pure water;
[0037] S3, when the reaction mixture ...
Embodiment 2
[0049]Embodiment 2 of the present invention discloses a method for efficiently preparing graphene, and the technical scheme adopted is as follows:
[0050] A method for efficiently preparing graphene, comprising the following steps:
[0051] S1, take 3g325 mesh natural flake graphite as raw material and 1.5g sodium nitrate, take an ice-water bath, add 150ml of concentrated sulfuric acid and stir for 60min at a stirring rate of 300-500rpm, add 12g potassium permanganate in batches to the mixed system, react for 100min, remove In an ice-water bath, the temperature was raised to 40°C, and the stirring reaction was continued for 2 hours;
[0052] S2, remove the reaction mixture obtained in step S1 from the water bath, cool to room temperature, stir and slowly add 90ml of pure water to dilute, control the temperature at 90°C for 30min, cool the reaction system naturally, lower the temperature to 50°C, stir and add 200ml at a temperature of 50°C of pure water;
[0053] S3, when th...
Embodiment 3
[0058] Embodiment 3 of the present invention discloses a kind of method for efficiently preparing graphene, and the technical scheme adopted is as follows:
[0059] A method for efficiently preparing graphene, comprising the following steps:
[0060] S1, take 10g of 100-mesh expandable graphite as raw material and expand graphite obtained by thermal expansion and 40g of sodium nitrate, take an ice-water bath, add 500ml of concentrated sulfuric acid and concentrated phosphoric acid and stir for 60min at a stirring rate of 300-500rpm. The volume ratio of concentrated phosphoric acid is 9:1, add 50g of potassium permanganate in batches to the mixed system, react for 120min, remove the ice-water bath, raise the temperature to 50°C, and continue stirring for 2.5h;
[0061] S2, remove the reaction mixture obtained in step S1 from the water bath, cool to room temperature, stir and slowly add 400ml of pure water to dilute, control the temperature at 90°C for 40min, cool the reaction s...
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