Conductive concrete for tower grounding and preparation method thereof
A technology of conductive concrete and pole towers, which is applied in the field of grounding material preparation, can solve the problems of increased volume resistivity of cement-based composite materials, poor conductivity improvement effect, and further improvement of conductivity, so as to achieve impermeability and frost resistance Good economical performance, improved compactness and mechanical properties, and strong plasticity
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Embodiment 1
[0030] (1) Preparation of polyaniline / bentonite composite material:
[0031] Weigh bentonite and cetyltrimethylammonium bromide according to a mass ratio of 5:1, dissolve in distilled water, soak statically at 80°C for 72h, filter, dry at 60°C, grind and sieve;
[0032] Prepare the hydrochloric acid solution of 2mol / L and the ammonium persulfate solution of 2mol / L, take quantitative bentonite through the above-mentioned organic treatment, add in the three-necked flask, pass into nitrogen in the three-necked flask, add aniline, hydrochloric acid solution successively, in Add ammonium persulfate dropwise under magnetic stirring at 15°C, and control the molar ratio n (aniline): n (hydrochloric acid): n (ammonium persulfate) = 1:0.5:1. After the reaction is complete, pour the obtained dark green mixture into In a G4 funnel, wash with distilled water until the filtrate becomes colorless; dry the filtered and washed powder at 60°C for 48 hours, and grind it into a fine powder in a m...
Embodiment 2
[0038] (1) Preparation of polyaniline / bentonite composite material:
[0039] Weigh bentonite and cetyltrimethylammonium bromide according to a mass ratio of 5:1, dissolve in distilled water, soak statically at 80°C for 72h, filter, dry at 60°C, grind and sieve;
[0040] Prepare the hydrochloric acid solution of 2mol / L and the ammonium persulfate solution of 2mol / L, take quantitative bentonite through the above-mentioned organic treatment, add in the three-necked flask, pass into nitrogen in the three-necked flask, add aniline, hydrochloric acid solution successively, in Add ammonium persulfate dropwise under magnetic stirring at 20°C, and control the molar ratio n (aniline): n (hydrochloric acid): n (ammonium persulfate) = 1:0.5:1. After the reaction is complete, pour the obtained dark green mixture into In a G4 funnel, wash with distilled water until the filtrate becomes colorless; dry the filtered and washed powder at 60°C for 48 hours, and grind it into a fine powder in a mor...
Embodiment 3
[0046] (1) Preparation of polyaniline / bentonite composite material:
[0047] Weigh bentonite and cetyltrimethylammonium bromide according to a mass ratio of 5:1, dissolve in distilled water, soak statically at 80°C for 72h, filter, dry at 60°C, grind and sieve;
[0048] Prepare the hydrochloric acid solution of 2mol / L and the ammonium persulfate solution of 2mol / L, take quantitative bentonite through the above-mentioned organic treatment, add in the three-necked flask, pass into nitrogen in the three-necked flask, add aniline, hydrochloric acid solution successively, in Add ammonium persulfate dropwise under magnetic stirring at 10°C, and control the molar ratio n (aniline): n (hydrochloric acid): n (ammonium persulfate) = 1:0.5:1. After the reaction is complete, pour the obtained dark green mixture into In a G4 funnel, wash with distilled water until the filtrate becomes colorless; dry the filtered and washed powder at 60°C for 48 hours, and grind it into a fine powder in a m...
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