Method for preparing anti-wrinkle regenerated silk by using defective silkworm cocoons
A regenerated silk, anti-wrinkle technology, applied in rayon manufacturing, textile and papermaking, chemical post-processing of fibers, etc., can solve the problems of affecting quality and aesthetics, unfavorable processing and use, poor quality of cocoons, etc., to avoid easy fading and uneven coloring, improving the degree of maturation, and improving the effect of emulsification
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Embodiment 1
[0023] A method for making anti-wrinkle regenerated silk by using defective silk cocoons, comprising the following steps:
[0024] (1) Pre-treatment: cut the defective silk cocoon and take out the silkworm chrysalis, wash it with water, and then micronize it to obtain cocoon micropowder, then use sodium hypochlorite solution to soak the cocoon micropowder for 22 minutes, and use the ventilation tube to introduce air to the bottom, filter and bake. dry, to obtain pre-treated cocoon powder;
[0025] (2) Silk dissolution: add deionized water and zeolite particles to the pre-treated silkworm cocoon micropowder, cook under high pressure for 38 minutes, filter after cooling, and add a mixed enzyme agent with 2.7% deionized water quality to it, and keep the temperature in a reaction kettle at 37°C Enzymatic hydrolysis for 3.5 hours to obtain silkworm cocoon enzymatic hydrolysis solution; heat silkworm cocoon enzymatic hydrolysis solution to 83°C, slowly add sodium hydroxide solution ...
Embodiment 2
[0040] A method for making wrinkle-resistant regenerated silk by using inferior silk cocoons, comprising the following steps:
[0041] (1) Pretreatment: Cut the defective silkworm cocoons to take out the silkworm chrysalis, wash with clean water and then micronize to obtain the silkworm cocoon micropowder, and then use the sodium hypochlorite solution to soak the silkworm cocoon micropowder for 26 minutes, and use the ventilation pipe to introduce air to the bottom, filter and bake the powder. Dry, get pre-treated silkworm cocoon powder;
[0042] (2) Silk dissolution: Add deionized water and zeolite particles to the pre-treated silkworm cocoon powder for high-pressure cooking for 44 minutes, filter after cooling, add a mixed enzyme agent with a mass of 3.7% deionized water to it, and keep it in a 41 ℃ reactor at a constant temperature Enzymatic hydrolysis was carried out for 4 hours to obtain cocoon enzymatic hydrolysis solution; the silkworm cocoon enzymatic hydrolysis soluti...
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