PVC pipe material and preparation method thereof
A PVC pipe and raw material technology, applied in the field of PVC pipe and its preparation, can solve the problems of structural strength, low stability, poor corrosion resistance and impact resistance, poor performance stability, etc., and achieve no equipment dependence High, excellent aging resistance, good strength and toughness
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Embodiment 1
[0030] A PVC pipe made of the following raw materials in parts by weight: 100 parts of polyvinyl chloride, 20 parts of polyfluorinated tertiary aminoterephthalic acid 1,1'-dianamantane-3,3'-diamine amide, 20 parts of carboxyl 10 parts of nitrile rubber, 5 parts of surface modified glass fiber, 5 parts of chlorinated polyethylene, 3 parts of lubricant PA20.
[0031] The preparation method of the polyfluorine-containing tertiary aminoterephthalic acid 1,1'-diamantane-3,3'-diamine amide comprises the following steps:
[0032] Step S1, add 1kg of 2-aminoterephthalic acid, 2.15kg of 1-chloromethyl-3-trifluoromethylbenzene, and 0.3kg of sodium hydroxide into acetonitrile, stir and react at 40°C for 4 hours, and then filter Remove insoluble matter, remove acetonitrile by rotary evaporation, then add dichloromethane and water to the reaction system for liquid separation, take the organic phase, remove water with anhydrous magnesium sulfate, filter and remove dichloromethane by rotary ...
Embodiment 2
[0037] A PVC pipe made of the following raw materials in parts by weight: 100 parts of polyvinyl chloride, 23 parts of polyfluorinated tertiary aminoterephthalic acid 1,1'-dianamantane-3,3'-diamine amide, 23 parts of carboxyl 11 parts of nitrile rubber, 6 parts of surface modified glass fiber, 6 parts of chlorinated polyethylene, 4 parts of lubricant P551A.
[0038] The preparation method of the polyfluorine-containing tertiary aminoterephthalic acid 1,1'-diamantane-3,3'-diamine amide comprises the following steps:
[0039] Step S1, add 1kg of 2-aminoterephthalic acid, 2.15kg of 1-chloromethyl-3-trifluoromethylbenzene, and 0.4kg of potassium hydroxide into 12kg of chloroform, stir and react at 45°C for 4.5 hours, and then Remove insoluble matter by filtration, remove chloroform by rotary evaporation, then add dichloromethane and water to the reaction system for liquid separation, take the organic phase, remove water with anhydrous magnesium sulfate, remove dichloromethane by r...
Embodiment 3
[0044] A PVC pipe made of the following raw materials in parts by weight: 100 parts of polyvinyl chloride, 25 parts of polyfluorinated tertiary aminoterephthalic acid 1,1'-dianamantane-3,3'-diamine amide, 25 parts of carboxyl 13 parts of nitrile rubber, 7.5 parts of surface modified glass fiber, 7.5 parts of chlorinated polyethylene, 5 parts of lubricant AC-316A.
[0045] The preparation method of the polyfluorine-containing tertiary aminoterephthalic acid 1,1'-diamantane-3,3'-diamine amide comprises the following steps:
[0046] Step S1, add 1kg of 2-aminoterephthalic acid, 2.15kg of 1-chloromethyl-3-trifluoromethylbenzene, and 0.45kg of sodium carbonate into 13.5kg of acetone, stir and react at 50°C for 5 hours, and then Remove the insoluble matter by filtration, remove the organic solvent by rotary evaporation, then add dichloromethane and water to the reaction system for liquid separation, take the organic phase, remove water with anhydrous magnesium sulfate, remove the di...
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