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PVC pipe material and preparation method thereof

A PVC pipe and raw material technology, applied in the field of PVC pipe and its preparation, can solve the problems of structural strength, low stability, poor corrosion resistance and impact resistance, poor performance stability, etc., and achieve no equipment dependence High, excellent aging resistance, good strength and toughness

Inactive Publication Date: 2019-09-24
徐海松
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The main purpose of the present invention is to provide a PVC pipe, which overcomes the more or less poor corrosion resistance and impact resistance of traditional PVC pipes, poor performance stability, and low structural strength and stability. Poor anti-aging performance, complex manufacturing process, low production pass rate, short service life, high cost, long production cycle, low production efficiency technical problems, have more excellent aging resistance, corrosion resistance, higher mechanical strength and Toughness, better impact resistance, better strength and toughness, longer service life, safer and more environmentally friendly use; at the same time, the invention also provides a preparation method for the PVC pipe

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] A PVC pipe made of the following raw materials in parts by weight: 100 parts of polyvinyl chloride, 20 parts of polyfluorinated tertiary aminoterephthalic acid 1,1'-dianamantane-3,3'-diamine amide, 20 parts of carboxyl 10 parts of nitrile rubber, 5 parts of surface modified glass fiber, 5 parts of chlorinated polyethylene, 3 parts of lubricant PA20.

[0031] The preparation method of the polyfluorine-containing tertiary aminoterephthalic acid 1,1'-diamantane-3,3'-diamine amide comprises the following steps:

[0032] Step S1, add 1kg of 2-aminoterephthalic acid, 2.15kg of 1-chloromethyl-3-trifluoromethylbenzene, and 0.3kg of sodium hydroxide into acetonitrile, stir and react at 40°C for 4 hours, and then filter Remove insoluble matter, remove acetonitrile by rotary evaporation, then add dichloromethane and water to the reaction system for liquid separation, take the organic phase, remove water with anhydrous magnesium sulfate, filter and remove dichloromethane by rotary ...

Embodiment 2

[0037] A PVC pipe made of the following raw materials in parts by weight: 100 parts of polyvinyl chloride, 23 parts of polyfluorinated tertiary aminoterephthalic acid 1,1'-dianamantane-3,3'-diamine amide, 23 parts of carboxyl 11 parts of nitrile rubber, 6 parts of surface modified glass fiber, 6 parts of chlorinated polyethylene, 4 parts of lubricant P551A.

[0038] The preparation method of the polyfluorine-containing tertiary aminoterephthalic acid 1,1'-diamantane-3,3'-diamine amide comprises the following steps:

[0039] Step S1, add 1kg of 2-aminoterephthalic acid, 2.15kg of 1-chloromethyl-3-trifluoromethylbenzene, and 0.4kg of potassium hydroxide into 12kg of chloroform, stir and react at 45°C for 4.5 hours, and then Remove insoluble matter by filtration, remove chloroform by rotary evaporation, then add dichloromethane and water to the reaction system for liquid separation, take the organic phase, remove water with anhydrous magnesium sulfate, remove dichloromethane by r...

Embodiment 3

[0044] A PVC pipe made of the following raw materials in parts by weight: 100 parts of polyvinyl chloride, 25 parts of polyfluorinated tertiary aminoterephthalic acid 1,1'-dianamantane-3,3'-diamine amide, 25 parts of carboxyl 13 parts of nitrile rubber, 7.5 parts of surface modified glass fiber, 7.5 parts of chlorinated polyethylene, 5 parts of lubricant AC-316A.

[0045] The preparation method of the polyfluorine-containing tertiary aminoterephthalic acid 1,1'-diamantane-3,3'-diamine amide comprises the following steps:

[0046] Step S1, add 1kg of 2-aminoterephthalic acid, 2.15kg of 1-chloromethyl-3-trifluoromethylbenzene, and 0.45kg of sodium carbonate into 13.5kg of acetone, stir and react at 50°C for 5 hours, and then Remove the insoluble matter by filtration, remove the organic solvent by rotary evaporation, then add dichloromethane and water to the reaction system for liquid separation, take the organic phase, remove water with anhydrous magnesium sulfate, remove the di...

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PUM

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Abstract

The invention provides a PVC pipe material. The PVC pipe material is characterized by being prepared from the following raw materials in parts by weight: 100 parts of polyvinyl chloride, 20 to 30 parts of polyfluoro tert-amino terephthalic acid 1,1'-biadamantane-3,3'-diamine amide, 10 to 15 parts of carboxyl nitrile rubber, 5 to 10 parts of surface-modified glass fiber, 5 to 10 parts of chlorinated polyethylene and 3 to 7 parts of a lubricant. The invention also discloses a preparation method for the PVC pipe material. The PVC pipe material disclosed by the invention has more excellent aging resistance and corrosion resistance, higher mechanical strength and toughness, more excellent impact resistance, better strength and toughness and longer service life, and is safer and more environmentally friendly to use.

Description

technical field [0001] The invention relates to the technical field of polymer materials, in particular to a PVC pipe and a preparation method thereof. Background technique [0002] In recent years, with the development of production and technology in the chemical and plastic industries, PVC pipes have excellent flame retardancy, wear resistance, chemical corrosion resistance, comprehensive mechanical properties, product transparency, electrical insulation and easier processing, etc. Features, are widely used in industry, construction, agriculture, daily life, packaging, electric power, public utilities and other fields. The development of PVC pipes with excellent performance meets market demand and has extensive social and economic value. [0003] The PVC pipes in the prior art have poor impact resistance due to the poor impact resistance of the pure PVC material itself, especially the poor low-temperature impact resistance, which limits its application in many fields. At ...

Claims

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Application Information

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IPC IPC(8): C08L27/06C08L77/06C08L13/00C08L23/28C08K9/06C08K7/14C08G69/42
CPCC08G69/42C08L27/06C08L2201/04C08L2201/08C08L2203/18C08L2205/035C08L77/06C08L13/00C08L23/286C08K9/06C08K7/14
Inventor 徐海松
Owner 徐海松
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