Production process of anti-bacterial environment-friendly anti-counterfeiting aluminum foil paper
A production process and technology of aluminum foil paper, applied in papermaking, fungicides, packaging paper, etc., can solve the problems of high cost, environmental pollution, complex recycling process, etc., and achieve the effect of cost and process saving, cost saving, and simple recycling
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Embodiment 1
[0023] The concrete preparation process of antibacterial discoloration colloid is as follows:
[0024] Step 1: Weigh 1 kg of pentanedione and add it to the reaction container, add 6 L of ethanol solution to it at the same time, stir and dissolve it, then add sodium hydroxide dropwise therein to adjust the pH of the solution to 13, and then add 560 g of acrolein to the reaction container, Stir the reaction at room temperature for 5-6 hours, then heat to 70°C and evaporate for 4-5 hours to remove the ethanol solvent and unreacted acrolein, then add dilute hydrochloric acid to the obtained product dropwise to adjust the pH of the product to 7, then adjust the acidity The adjusted product was extracted with ether, and the upper oil phase was collected and then subjected to vacuum distillation to obtain dialdehyde diketone;
[0025] Step 2: Weigh 1 kg of 2,4-dinitrophenylhydrazine and add it to 10 L of acetic acid solution, cool it down to 5-10° C. and stir to dissolve, then add 65...
Embodiment 2
[0035] The concrete preparation process of antibacterial discoloration colloid is as follows:
[0036] Step 1: Weigh 1 kg of pentanedione and add it to the reaction container, add 6 L of ethanol solution to it at the same time, stir and dissolve it, then add sodium hydroxide dropwise therein to adjust the pH of the solution to 13, and then add 560 g of acrolein to the reaction container, Stir the reaction at room temperature for 5-6 hours, then heat to 70°C and evaporate for 4-5 hours to remove the ethanol solvent and unreacted acrolein, then add dilute hydrochloric acid to the obtained product dropwise to adjust the pH of the product to 7, then adjust the acidity The adjusted product was extracted with ether, and the upper oil phase was collected and then subjected to vacuum distillation to obtain dialdehyde diketone;
[0037] Step 2: Weigh 1 kg of 2,4-dinitrophenylhydrazine and add it to 10 L of acetic acid solution, cool it down to 5-10° C. and stir to dissolve, then add 65...
Embodiment 3
[0041] The concrete preparation process of antibacterial discoloration colloid is as follows:
[0042] Step 1: Weigh 1 kg of pentanedione and add it to the reaction container, add 6 L of ethanol solution to it at the same time, stir and dissolve, add 4.5 kg of saturated sodium sulfate solution to it, stir and react for 5-7 hours at room temperature, and then evaporate to remove the solvent Water and ethanol, adding the solid product into ethanol, stirring and mixing, filtering, collecting the filtrate and carrying out vacuum distillation to obtain dihydroxy sodium bisulfite;
[0043] Step 2: Add 1kg of polyvinyl alcohol with a low degree of polymerization into 8L of hot water at 65-70°C and stir to dissolve, then add 0.431kg of the dihydroxy sodium bisulfite prepared in step 2, stir to dissolve, and then drop by drop Add 0.126kg of toluene diisocyanate, control the dropping rate to 8-9mL / min, stir and react at a constant temperature for 4-5h after the dropping is complete, and...
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