Composite polyester filament and processing method thereof
A technology of polyester filament and processing method, which is applied in filament/thread forming, melting of filament raw materials, and manufacture of fire-resistant and flame-retardant filaments. It can solve problems such as poor layering and single flame-retardant effect, and achieve improved dispersion properties, avoiding the loss of flame retardant performance, and the effect of high phosphorus content
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Embodiment 1
[0053] A composite polyester filament with a flame-retardant property of LOI of 31%, a fineness of 0.20dpf, a breaking strength of 3.3cN / dtex, and a breaking elongation of 20%.
[0054] A processing method for composite polyester filament, the concrete steps are:
[0055] (1) Preparation of molten phosphorus-containing flame retardant:
[0056] Using furandicarbaldehyde and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxa (DOPO) as raw materials, firstly DOPO was dissolved in dichloroethane, and then under nitrogen protection, the furan The dichloroethane solution of diformaldehyde was added to the reaction system, and then refluxed at 60-80°C for 12 hours to obtain a white powder precipitate. Vacuum drying for 24 hours to prepare a molten phosphorus-containing flame retardant;
[0057] The phosphorus content of the molten phosphorus-containing flame retardant is 11.5 wt%, and the melting point of the molten phosphorus-containing flame retardant is 156-160°C.
[0058] The m...
Embodiment 2
[0070] A composite polyester filament with a flame-retardant property of LOI of 32%, a fineness of 2dpf, a breaking strength of 3.5cN / dtex, and a breaking elongation of 30%.
[0071] A processing method for composite polyester filament, the concrete steps are:
[0072] (1) Preparation of molten phosphorus-containing flame retardant:
[0073] Using furandicarbaldehyde and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxa (DOPO) as raw materials, firstly DOPO was dissolved in dichloroethane, and then under nitrogen protection, the furan The dichloroethane solution of diformaldehyde was added to the reaction system, and then refluxed at 60-80°C for 12 hours to obtain a white powder precipitate. Vacuum drying for 24 hours to prepare a molten phosphorus-containing flame retardant;
[0074] The phosphorus content of the molten phosphorus-containing flame retardant is 11.6 wt%, and the melting point of the molten phosphorus-containing flame retardant is 156-160°C.
[0075] The mass...
Embodiment 3
[0086] A composite polyester filament with a flame-retardant property of LOI of 33%, a fineness of 3.3dpf, a breaking strength of 4.0cN / dtex, and a breaking elongation of 45%.
[0087] A processing method for composite polyester filament, the concrete steps are:
[0088] (1) Preparation of molten phosphorus-containing flame retardant:
[0089] Using furandicarbaldehyde and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxa (DOPO) as raw materials, firstly DOPO was dissolved in dichloroethane, and then under nitrogen protection, the furan The dichloroethane solution of diformaldehyde was added to the reaction system, and then refluxed at 60-80°C for 12 hours to obtain a white powder precipitate. Vacuum drying for 24 hours to prepare a molten phosphorus-containing flame retardant;
[0090] The phosphorus content of the molten phosphorus-containing flame retardant is 11.8 wt%, and the melting point of the molten phosphorus-containing flame retardant is 156-160°C.
[0091] Descri...
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