Aluminum ion electrolyte solution, magnesium ion electrolyte solution and battery
An electrolyte solution and aluminum ion technology, applied in the energy field, can solve the problems of price reversal, resource shortage, etc., and achieve the effects of high cost performance, excellent safety, and rapid charge and discharge.
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[0036] The preparation method of the carbon-sulfur intermolecular compound electrode comprises the following steps:
[0037]1) Mix microcrystalline graphite or conductive carbon black with a particle size of less than 500 mesh and sulfur evenly in a ratio of carbon to sulfur weight ratio equal to 1:0.7 to 1:0.5, fill it into an autoclave with an air extraction device and compact it.
[0038] There is no strict stoichiometric ratio for the formation of intermolecular compounds between carbon and sulfur, and the recommended carbon-sulfur ratio is an optimized empirical value. Products synthesized with higher carbon-sulfur ratios have better conductivity, but relatively lower energy density; products synthesized with lower carbon-sulfur ratios have lower conductivity, but higher energy density.
[0039] 2) Connect the exhaust valve of the autoclave to the vacuum pump, and close the exhaust valve after vacuuming.
[0040] The purpose of vacuuming the autoclave is to ensure safety...
Embodiment 1
[0078] Mix aluminum trifluoromethanesulfonate and sodium hexafluorophosphate at a weight ratio of 1:1, then add ethyl methyl carbonate solvent 3 times the weight of the solid, stir until the solid is completely dissolved, and heat to a constant temperature of 110°C Water was removed for 8 hours to obtain an aluminum ion electrolyte solution.
Embodiment 2
[0080]Mix aluminum trifluoromethanesulfonate and sodium hexafluorophosphate at a weight ratio of 1:1.5, then add gamma-butyrolactone solvent 5 times the weight of the solid, stir until the solid is completely dissolved, and heat to 130°C Constant temperature for 5 hours to remove moisture, to aluminum ion electrolyte solution. An aluminum ion electrolyte solution is obtained.
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