Substrate-supported functionalized conducting polymer film and preparation method thereof
A conductive polymer, functionalization technology, applied to the conductive layer on the insulating carrier, equipment for manufacturing conductive/semiconductive layer, conductive material, etc., can solve the complex preparation method, poor uniformity of conductive polymer film, film Unable to control the thickness and other problems, to achieve the effect of expanding the application range, low cost and high selectivity
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Embodiment 1
[0031] A functionalized conductive polymer film supported by a substrate is composed of a substrate and a functionalized conductive polymer film deposited on its surface, and its preparation steps are as follows:
[0032] (1) Drying after cleaning the silicon dioxide sheet: washing with detergent, deionized water, acetone, dichloromethane and isopropanol in sequence under the action of ultrasound, and the washing time (t1) for each time is 15 minutes;
[0033] (2) FeCl 3 The solution was dropped on a silica wafer, and FeCl was obtained by spin-coating method 3 Membrane, rotating speed is 6000rpm, time is 60s; Among them, FeCl 3 The mass concentration (c) of solution is 7wt%, and solvent is n-butanol, FeCl 3 The thickness (h1) of the film is 103 nm;
[0034] (3) will be coated with FeCl 3The silicon dioxide sheet of the film and the functionalized monomer (M-1) were placed in a vapor deposition polymerization furnace, deposited and polymerized at a temperature (T) of 80°C, ...
Embodiment 2～15
[0038] A substrate-supported functionalized conductive polymer film, the preparation method of Examples 2-15 is basically the same as that of Example 1, the difference is that the parameters in the preparation process are different, see Table 1 for details, wherein, M represents functionalized conductive Polymer, see Table 2 specifically, the performance index of the functionalized conductive polymer film of the substrate support that makes is shown in Table 3, wherein, select the polymer film of embodiment 3 to carry out infrared spectrum test, select the polymer film of embodiment 5 for use Carry out Raman spectroscopy test, the results are as follows figure 1 and figure 2 Shown; Select the polymer film of embodiment 2 to carry out resistance test, and its result is as follows image 3 shown.
[0039] The preparation parameter of table 1 embodiment 2~15
[0040]
[0041]
[0042] Table 2 The number and molecular formula of the functionalized conductive polymer mono...
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Abstract
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