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Method for preparing herbicide from Jatropha curcas plant residues

A technology for plant residues and herbicides, applied in the directions of botanical equipment and methods, chemicals for biological control, plant growth regulators, etc. The effect of activity, simple process and low cost

Inactive Publication Date: 2020-01-10
凉山德农生物能源股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] On the other hand, in the process of agricultural production, the growth of weeds competes with crops for nutrients, spreads diseases and insect pests, and reduces agricultural production efficiency. However, the extensive use of chemical herbicides also leads to environmental pollution and the emergence of drug-resistant weeds. Low-toxic and cheap bio-pesticides are the inevitable trend of today's agricultural production
At present, there are few reports on the development of herbicides from Jatropha jatropha extracts. This patent utilizes the biological toxicity of toxic proteins and alkaloids contained in it to prepare environmentally friendly and efficient biological herbicides

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] Get 0.3kg Jatropha leaf fragments, 0.6kg Jatropha twig fine sawdust, and 1kg Jatropha husk debris, disperse them in 15L of 5% acetic acid solution, and perform ultrasonic treatment while stirring at room temperature. The ultrasonic power is 300W. The time is 30 minutes. After the treatment, suction filtration under reduced pressure was carried out at 0.05Mpa to obtain a yellow aqueous phase. Repeat the above steps twice to obtain about 25L of aqueous extract. Add 10 L of ethyl acetate to the residue left in the above process, and conduct continuous extraction at 80° C. for 4 hours to obtain about 10 L of yellow organic phase extract. Take 25L of the aqueous phase extract and 10L of the organic phase extract and mix them at 40°C and 0.05kpa for vacuum distillation to remove water and ethyl acetate to obtain a brown viscous extract.

[0030] Take 5 g of yellow viscous crude extract, add 100 g of dextrin, add 150 mL of water, stir the mixture evenly, and dry granulate to...

Embodiment 2

[0032] Get 0.5kg Jatropha leaf fragments, 0.5kg Jatropha twig fine sawdust, 0.5kg part Jatropha husk debris, be dispersed in 5% acetic acid solution of 10L, under room temperature, ultrasonic treatment while stirring, the power of ultrasonic is 200W, Ultrasonic time 40min. After the treatment, suction filtration under reduced pressure was carried out at 0.01Mpa to obtain a yellow aqueous phase. Repeat the above steps twice to obtain about 15 L of aqueous extract. Add 10 L of ethyl acetate to the residue left in the above process, and conduct continuous extraction at 80° C. for 2 hours to obtain about 9 L of yellow organic phase extract. Take 15L of the aqueous phase extract and 9L of the organic phase extract and mix them at 38°C and 0.04kpa for vacuum distillation to remove water and ethyl acetate to obtain a brown viscous crude extract.

[0033] Take 2g of the brown viscous extract, add 100g of kaolin, add 100mL of water, stir the mixture evenly, and prepare a commercial w...

Embodiment 3

[0035] Get 0.5kg Jatropha leaf fragments, 0.5kg Jatropha twig fine sawdust, and 2kg parts Jatropha husk debris, disperse them in 30L of 5% acetic acid solution, and ultrasonicate while stirring at room temperature. The ultrasonic power is 500W. The time is 60 minutes. After the treatment, suction filtration under reduced pressure was carried out at 0.1Mpa to obtain a yellow aqueous phase. Repeat the above steps twice to obtain about 55L of aqueous extract. 20L of dichloromethane was added to the residue left in the above process, and after continuous extraction at 50°C for 6 hours, about 20L of yellow organic phase extract was obtained. Take 55L of the aqueous phase extract and 20L of the organic phase extract and mix them at 30°C and 0.01kpa for vacuum distillation to remove water and dichloromethane to obtain a brown viscous crude extract.

[0036] Take 8g of brown viscous crude extract, 100g of bentonite, add 500mL of water, stir well, then evaporate the mixture to drynes...

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PUM

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Abstract

The invention provides a method for preparing a herbicide from Jatropha curcas plant residues, and belongs to the technical field of herbicides. The method comprises the following steps: taking 0.3-1kg of Jatropha curcas leaf fragments, 0.3-1 kg of Jatropha curcas branch fine wood chips and 0.3-2 kg of Jatropha curcas shell fragments, dispersing the taken materials in 15-30 L of an acetic acid solution, and carrying out ultrasonic treatment while stirring at the room temperature; carrying out natural filtering or vacuum filtration to remove residues in order to obtain a yellow water phase; repeating above the above steps for 3-5 times, mixing the yellow water phases obtained each time to obtain a water phase extract, and mixing residues obtained each time; adding the filtered residues to10-20 L of a low-boiling-point organic solvent, and carrying out reflux continuous extraction to obtain an organic phase extract; and mixing the water-phase extract with the organic-phase extract according to a volume ratio of (2-4):1, carrying out reduced pressure distillation, and recovering the organic solvent and water to obtain a brown viscous extract that is the herbicide.

Description

technical field [0001] The invention belongs to the technical field of herbicides, and in particular relates to a method for preparing herbicides by using jatropha plant residues. Background technique [0002] Jatropha curcas L. is a Euphorbiaceae shrub native to tropical America. Studies have shown that the oil content of the fruit of this tree species can be as high as 60%. In terms of medicinal value, the leaves of Jatropha curcas can be used as medicine to treat bruises, fractures, eczema and digestive tract inflammation. Generally speaking, Jatropha has important economic value, and it has been planted on a large scale in Panxi and Yunnan in my country. Relying on Jatropha plantation industry to produce biodiesel with higher added value and produce Chinese herbal decoction pieces has become one of the effective ways for local farmers to get rid of poverty and become rich. [0003] Modern research shows that the active ingredients contained in Jatropha are relatively c...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N65/18A01P13/00
CPCA01N65/00A01N65/18
Inventor 曾伟赵丽娟易龙飞宋永娇高元吉史英博张欣汝
Owner 凉山德农生物能源股份有限公司
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