Method for preparing herbicide from Jatropha curcas plant residues
A technology for plant residues and herbicides, applied in the directions of botanical equipment and methods, chemicals for biological control, plant growth regulators, etc. The effect of activity, simple process and low cost
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Embodiment 1
[0029] Get 0.3kg Jatropha leaf fragments, 0.6kg Jatropha twig fine sawdust, and 1kg Jatropha husk debris, disperse them in 15L of 5% acetic acid solution, and perform ultrasonic treatment while stirring at room temperature. The ultrasonic power is 300W. The time is 30 minutes. After the treatment, suction filtration under reduced pressure was carried out at 0.05Mpa to obtain a yellow aqueous phase. Repeat the above steps twice to obtain about 25L of aqueous extract. Add 10 L of ethyl acetate to the residue left in the above process, and conduct continuous extraction at 80° C. for 4 hours to obtain about 10 L of yellow organic phase extract. Take 25L of the aqueous phase extract and 10L of the organic phase extract and mix them at 40°C and 0.05kpa for vacuum distillation to remove water and ethyl acetate to obtain a brown viscous extract.
[0030] Take 5 g of yellow viscous crude extract, add 100 g of dextrin, add 150 mL of water, stir the mixture evenly, and dry granulate to...
Embodiment 2
[0032] Get 0.5kg Jatropha leaf fragments, 0.5kg Jatropha twig fine sawdust, 0.5kg part Jatropha husk debris, be dispersed in 5% acetic acid solution of 10L, under room temperature, ultrasonic treatment while stirring, the power of ultrasonic is 200W, Ultrasonic time 40min. After the treatment, suction filtration under reduced pressure was carried out at 0.01Mpa to obtain a yellow aqueous phase. Repeat the above steps twice to obtain about 15 L of aqueous extract. Add 10 L of ethyl acetate to the residue left in the above process, and conduct continuous extraction at 80° C. for 2 hours to obtain about 9 L of yellow organic phase extract. Take 15L of the aqueous phase extract and 9L of the organic phase extract and mix them at 38°C and 0.04kpa for vacuum distillation to remove water and ethyl acetate to obtain a brown viscous crude extract.
[0033] Take 2g of the brown viscous extract, add 100g of kaolin, add 100mL of water, stir the mixture evenly, and prepare a commercial w...
Embodiment 3
[0035] Get 0.5kg Jatropha leaf fragments, 0.5kg Jatropha twig fine sawdust, and 2kg parts Jatropha husk debris, disperse them in 30L of 5% acetic acid solution, and ultrasonicate while stirring at room temperature. The ultrasonic power is 500W. The time is 60 minutes. After the treatment, suction filtration under reduced pressure was carried out at 0.1Mpa to obtain a yellow aqueous phase. Repeat the above steps twice to obtain about 55L of aqueous extract. 20L of dichloromethane was added to the residue left in the above process, and after continuous extraction at 50°C for 6 hours, about 20L of yellow organic phase extract was obtained. Take 55L of the aqueous phase extract and 20L of the organic phase extract and mix them at 30°C and 0.01kpa for vacuum distillation to remove water and dichloromethane to obtain a brown viscous crude extract.
[0036] Take 8g of brown viscous crude extract, 100g of bentonite, add 500mL of water, stir well, then evaporate the mixture to drynes...
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