Solvent-free glazed finish-coat paint and preparation method thereof
A solvent-free, topcoat technology, used in biocide-containing paints, coatings, antifouling/underwater coatings, etc., can solve the problems of poor color weather resistance, insufficient polishing mirror effect, etc., to achieve high gloss and fullness The effect of improving the mirror effect of imitation stone polishing, excellent weather resistance and bending flexibility
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[0043] Another aspect of the present invention provides the preparation method of the solvent-free glaze type finish paint described in any one of the above embodiments, including:
[0044] S10, preparation of mixed modified TDI prepolymer mixture: add solvent-free TDI prepolymer into the container, disperse at a medium speed of 500-800r / min, and add hydrogenated epoxy resin, coagent, defoaming agent in sequence agent, dispersing wetting agent and nano fumed silicon oxide, when adding nano fumed silicon oxide, adjust the rotation speed to high speed 800-1000r / min, disperse for 15-25 minutes, and then disperse at low speed 300-500r / min for 3-8min to obtain The mixed modified TDI prepolymer mixture with a viscosity of 5000-10000mpa.s;
[0045] S20, the preparation of the solvent-free glaze type finish paint, take the mixed modified TDI prepolymer mixture and the adduct of alicyclic amine according to the epoxy equivalent in the mixed modified TDI prepolymer mixture and the addit...
Embodiment 1
[0049] Provide a solvent-free glaze type finish, which is synthesized by mixing a modified TDI prepolymer mixture and an alicyclic amine adduct, the components contained in the mixed modified TDI prepolymer mixture and each component The weight is (based on the total weight of 100g):
[0050] TDI polyisocyanate prepolymer with blocked isocyanate 18.0
[0051]
[0052] Concrete preparation steps are:
[0053] S10, add TDI polyisocyanate prepolymer containing blocked isocyanate and hydrogenated epoxy resin into the container, and add coagent, defoamer, dispersing and wetting When adding nano fumed silica, adjust the speed of the disperser to a high speed of 800-1000r / min, disperse for 20 minutes and then disperse at a speed of 300-500r / min for 5 minutes to obtain a mixed modified TDI prepolymer body mixture;
[0054] S20, during construction and application, the ratio of the epoxy equivalent in the mixed modified TDI prepolymer mixture to the active hydrogen equivalent in ...
Embodiment 2
[0069] Provide a solvent-free glaze type finish, which is synthesized by mixing a modified TDI prepolymer mixture and an alicyclic amine adduct, the components contained in the mixed modified TDI prepolymer mixture and each component The weight is (based on the total weight of 100g):
[0070] TDI polyisocyanate prepolymer with blocked isocyanate 22.0
[0071]
[0072] Concrete preparation steps are:
[0073] S10, add TDI polyisocyanate prepolymer containing blocked isocyanate and hydrogenated epoxy resin into the container, and add coagent, defoaming agent 1, defoaming Agent 2, dispersing wetting agent and nano fumed silica, when adding nano fumed silica, adjust the speed of the disperser to a high speed of 800-1000r / min, disperse for 20 minutes, and then disperse at a speed of 300-500r / min for 5 minutes. Mixed modified TDI prepolymer mixture;
[0074] S20, during construction and application, the ratio of the epoxy equivalent in the mixed modified TDI prepolymer mixture...
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