Glass film and preparation method thereof
A glass film and modification technology, which is applied in the production of film/sheet adhesives, adhesives, bulk chemicals, etc., can solve problems affecting GPS satellite navigation system signal reception, signal interference, poor performance, etc. The effect of size controllable, prolonging the service life and improving the bonding fastness
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Example Embodiment
[0031] Example 1
[0032] A glass film, the glass film is composed of the following parts by weight of raw materials: 100 parts of modified PET resin, 7 parts of modified masterbatch, 0.8 parts of coupling agent and 2.5 parts of additives; the modified masterbatch is Benzimidazole dione compound and modified PET resin coat inorganic oxide solid particles.
[0033] The modified PET resin is a polyhydroxy cage silsesquioxane modified PET resin.
[0034] The cage silsesquioxane modified PET resin is prepared by adding polyhydroxy cage silsesquioxane to the raw materials of terephthalic acid and ethylene glycol for polycondensation reaction. The added amount of siloxane accounts for 5.5% by mass of the raw material.
[0035] The benzimidazole dione compound is 5-hydroxy-1,2,6-trimethyl-1H-benzimidazole-4,7-dione.
[0036] The inorganic oxide solid particles are titanium dioxide.
[0037] The particle size of the modified masterbatch is 300 nm.
[0038] The coupling agent is composed of sila...
Example Embodiment
[0044] Example 2
[0045] A glass film, the glass film is composed of the following parts by weight of raw materials: 100 parts of modified PET resin, 4 parts of modified masterbatch, 0.5 parts of coupling agent and 2 parts of additives; the modified masterbatch is Benzimidazole dione compound and modified PET resin coat inorganic oxide solid particles.
[0046] The modified PET resin is a polyhydroxy cage silsesquioxane modified PET resin.
[0047] The cage silsesquioxane-modified PET resin is prepared by adding polyhydroxy cage silsesquioxane to the raw materials of terephthalic acid and ethylene glycol for polycondensation reaction. The amount of siloxane added accounts for 3% by mass of the raw material.
[0048] The benzimidazole dione compound is 2-(hydroxymethyl)-1H-benzimidazole-4,7-dione.
[0049] The inorganic oxide solid particles are silica.
[0050] The particle size of the modified masterbatch is 100 nm.
[0051] The coupling agent is composed of silane coupling agent KH-5...
Example Embodiment
[0057] Example 3
[0058] A glass film, the glass film is composed of the following parts by weight of raw materials: 100 parts of modified PET resin, 12 parts of modified masterbatch, 1.0 part of coupling agent and 3 parts of additives; the modified masterbatch is Benzimidazole dione compound and modified PET resin coat inorganic oxide solid particles.
[0059] The modified PET resin is a polyhydroxy cage silsesquioxane modified PET resin.
[0060] The cage silsesquioxane-modified PET resin is prepared by adding polyhydroxy cage silsesquioxane to the raw materials of terephthalic acid and ethylene glycol for polycondensation reaction. The added amount of siloxane accounts for 8% by mass of the raw material.
[0061] The mass ratio of the benzimidazole dione compound is 1:1 5-hydroxy-1,2,6-trimethyl-1H-benzimidazole-4,7-dione and 2-(hydroxymethyl) -1H-benzimidazole-4,7-dione.
[0062] The inorganic oxide solid particles are composed of titanium dioxide and silicon dioxide with a mass...
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