Preparation method of high-viscosity durable plastering mortar
A high-viscosity technology for plastering mortar, which is applied in the field of building material preparation, can solve problems such as poor durability, cracking, and poor moisture-proof performance of plastering mortar, and achieve the effects of enhanced mechanical strength and thermal stability, improved durability, and enhanced moisture-proof performance
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Embodiment 1
[0033] Preparation of oxidation reaction solution:
[0034] Put bagasse and castor into an oven at a mass ratio of 5:1, dry for 100 minutes at a temperature of 70°C, and put them into a planetary ball mill after drying at a ball-to-material ratio of 10:1 and a rotational speed of 100r / min. Grind down for 30min to prepare the grinding mixture, and the grinding mixture and the mass fraction of 10% sodium hydroxide solution are thrown into the reactor in a mass ratio of 1:10;
[0035] Fill the reactor with ammonia until the pressure in the reactor rises to 0.8MPa, raise the temperature in the reactor to 150°C, react at constant temperature and pressure for 60 minutes, filter the filter residue after the reaction, wash the filter residue 3 times with distilled water, and put Put the filter residue and distilled water into a beaker at a mass ratio of 1:10, place the beaker in a resistance heating jacket, raise the temperature inside the heating jacket to 110°C, and heat at a consta...
Embodiment 2
[0043] Preparation of oxidation reaction solution:
[0044] Put bagasse and castor into an oven at a mass ratio of 5:1, dry for 110 minutes at a temperature of 75°C, and put them into a planetary ball mill after drying at a ball-to-material ratio of 10:1 and a speed of 110r / min. Grind down for 35min to prepare the grinding mixture, and the grinding mixture and the mass fraction of 12% sodium hydroxide solution are thrown into the reactor in a mass ratio of 1:10;
[0045] Fill the reactor with ammonia until the pressure in the reactor rises to 1.0MPa, raise the temperature in the reactor to 160°C, and react at constant temperature and pressure for 70 minutes. After the reaction, filter the residue and wash the residue with distilled water for 4 times. Put the filter residue and distilled water into a beaker at a mass ratio of 1:10, place the beaker in a resistance heating mantle, raise the temperature inside the heating mantle to 115°C, and heat at a constant temperature for 35...
Embodiment 3
[0053] Preparation of oxidation reaction solution:
[0054] Put bagasse and castor into an oven at a mass ratio of 5:1, dry for 120 minutes at a temperature of 80°C, and put them into a planetary ball mill after drying at a ball-to-material ratio of 10:1 and a rotational speed of 120r / min. Grind down for 30-40 minutes to prepare the grinding mixture, and put the grinding mixture and 15% sodium hydroxide solution into the reaction kettle at a mass ratio of 1:10;
[0055] Fill the reactor with ammonia until the pressure in the reactor rises to 1.2MPa, raise the temperature in the reactor to 170°C, and react at constant temperature and pressure for 80 minutes. After the reaction, filter the filter residue, wash the filter residue 5 times with distilled water, and Put the filter residue and distilled water into a beaker at a mass ratio of 1:10, place the beaker in a resistance heating jacket, raise the temperature inside the heating jacket to 120°C, and heat at a constant temperat...
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