Application and application method of foaming agent in prevention of coking and caking of organic matters during thermal decomposition
An application method and technology of organic matter, applied in the field of thermal decomposition of organic matter, can solve the problems of incomplete decomposition of organic matter, incomplete thermal decomposition, coking, etc., and achieve the effects of low cost, loose structure, and large tailing porosity
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Embodiment 1
[0027] A method for applying a blowing agent to anti-coking and agglomeration of organic matter thermal decomposition, comprising the following steps:
[0028] Take 2620 grams of oil sludge from the Liaohe Oilfield, and 13 grams of potassium stearate modified sodium bicarbonate foaming agent into the testing machine, heat the testing machine, and collect oil, water and steam. Heating started at 9:00 in the morning; at 9:15, the equipment was at 100°C, and a small amount of oil and water was discharged; at 9:55, the temperature was 200°C, and the oil and water continued to be discharged, and the discharged gas was flammable; at 10:25, the temperature was 450°C, and there was still oil vapor Discharge; 10:45 temperature 520 ℃, no oil vapor discharge; 11:10 stop heating.
[0029] The obtained various indicators of oil, water and residue are shown in Table 1:
[0030] Table 1
[0031] residue Oil water noncondensable gas Content of petroleum substances in tail ...
Embodiment 2
[0034] A method for applying a blowing agent to anti-coking and agglomeration of organic matter thermal decomposition, comprising the following steps:
[0035] Mix 2500g of waste engine oil regenerated residue with 25g of iron stearate modified sodium bicarbonate foaming agent into the furnace, and fasten the device;
[0036] Heating starts at 10:19 am;
[0037] 10:29 The temperature rises by 100°C, and no oil vapor is discharged;
[0038] 11:03 The temperature was 400°C, a large amount of gas and oil were discharged;
[0039] 11:30 When the temperature is 500°C, no oil vapor is discharged;
[0040] 11:35 Stop heating and let it cool down;
[0041] Experimental results: the oil production is 1600g, accounting for 64% of the total;
[0042] The various indicators of the obtained oil and residue are shown in Table 2
[0043] Table 2
[0044] Pink carbon Oil Non-condensable gases and impurities 32％ 64％ 4％
[0045] The gas is combustible; from the at...
Embodiment 3
[0047] A method for applying a blowing agent to anti-coking and agglomeration of organic matter thermal decomposition, comprising the following steps:
[0048] Add 1340g of drilling oil mud and 15g of sodium bicarbonate-silane coupling copolymer foaming agent into the furnace, and fasten the device;
[0049] Heating starts at 12:00 am;
[0050] 12:10 The temperature is 100°C, and the temperature of the high tower is 25°C;
[0051] 12:15 The temperature is 200°C, and the temperature of the high tower is 40°C;
[0052] 12:22 The temperature is 300°C, the temperature of the high tower is 50°C, the surface temperature of the outer wall of the furnace is 426°C, and a small amount of gas is discharged;
[0053] 12:32 The temperature is 400°C, the temperature of the high tower is 45°C, the gas is discharged, and a small amount of oil-water mixture is produced;
[0054] 12:40 The temperature is 450°C, the temperature of the high tower is 40°C, and the surface temperature of the out...
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