Heat-resistant and oil-resistant sealing ring and preparation method thereof
An oil-resistant sealing ring and heat-resistant technology, applied in the field of heat-resistant and oil-resistant sealing ring and its preparation
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[0037]The present invention also provides a method for preparing the above-mentioned heat-resistant and oil-resistant sealing ring, comprising the following steps:
[0038] 1) Nitrile rubber, chlorosulfonated polyethylene, vinyl trimethoxysilane, carbon black N330, filler, urethane, polyolefin elastomer, vinyl bis stearamide, diethyl disulfide Substitute zinc carbamate and anti-aging agent into the internal mixer and banbury at 80-100°C for 8-12 minutes;
[0039] 2) Put the rubber material well mixed into the open mill, and then add carbon black N330, 2,5-dimethyl-2,5-bis(tert-butylperoxy)hexane at 80 Mixing at ~120°C for 4-6 minutes, thinning and sheeting;
[0040] 3) Cut the film in step (3) into the required model products for production, heat the mold to 160-180°C with a vacuum flat vulcanizer, then put the cut film into the mold cavity, close the mold for vulcanization, and pressurize to 160~180Kgf / cm 2 Finally, the vulcanization time is 3 to 5 minutes, the product is ...
Embodiment 1
[0045] The preparation method of filler, comprises the following steps:
[0046] 1) After the filler is pulverized, it is divided into two parts, that is, the first filler and the second filler, for later use; the mass ratio of the first filler to the second filler is 1.3:1; the filler is aluminum hydroxide;
[0047] 2) Chitosan is added in the acetic acid solution, and stirred evenly, obtains the chitosan acetic acid solution;
[0048] 3) Add the first filler obtained in step 1) into the chitosan acetic acid solution and stir evenly, then add sodium hydroxide until the pH value reaches 6, and then stir for 80 minutes;
[0049] 4) Add the second filler to the mixture obtained in step 3), stir for 2 hours, filter and wash to obtain a filter cake, vacuum-dry the filter cake at 40° C., grind it, and pass through a 300-mesh sieve to obtain the filler.
Embodiment 2
[0051] The preparation method of filler, comprises the following steps:
[0052] 1) After the filler is pulverized, it is divided into two parts, that is, the first filler and the second filler, for later use; the mass ratio of the first filler to the second filler is 1.6:1; the filler is magnesium hydroxide and calcium carbonate, magnesium hydroxide and The mass ratio of calcium carbonate is 1:1;
[0053] 2) Chitosan is added in the acetic acid solution, and stirred evenly, obtains the chitosan acetic acid solution;
[0054] 3) Add the first filler obtained in step 1) into the chitosan acetic acid solution and stir evenly, then add sodium hydroxide until the pH value reaches 7, and then stir for 100 min;
[0055] 4) Add the second filler to the mixed solution obtained in step 3), stir for 3 hours, filter and wash to obtain a filter cake, vacuum-dry the filter cake at 60° C., grind it, and pass through a 500-mesh sieve to obtain the filler.
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