Method for preparing single-layer self-assembled porous film
A self-assembly, porous membrane technology, applied in chemical instruments and methods, membrane technology, semi-permeable membrane separation, etc., can solve the problems of low flux, large thickness of porous membrane membrane, etc. Small, cost-effective film production and fast results
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Embodiment 1
[0030] Apparatus for preparing thin films
[0031] The device includes a solution tank and a roller arranged in the solution tank, and the prepared single-layer self-assembled porous membrane moves from one end of the solution tank to the other end of the solution tank through the roller.
Embodiment 2
[0033] Preparation of polycaprolactone (PCL) film
[0034] Step S1: dissolving polycaprolactone with a molecular weight of 8K in dichloromethane to form a 2% w / v polymer homogeneous solution;
[0035] Step S2: loading the homogeneous polymer solution on a grid base, the grid base has a thickness of 50 μm, a pore diameter of 400 μm, and a line width of 50 μm, and the grid unit is a honeycomb through-hole membrane.
[0036] Step S3: Evaporate the solvent on the grid base with hot air, the temperature of the hot air is 22° C., the time of the hot air is 5 s, and the speed of the hot air is 3 m / s.
[0037] Step S4: After stopping the evaporation, a thin film is obtained.
Embodiment 3
[0039] Preparation of poly(lactic-co-glycolic acid) (PLGA) film
[0040] Step S1: dissolving PLGA with a molecular weight of 7.5K in dichloromethane to form a 2% w / v homogeneous polymer solution;
[0041] Step S2: loading the homogeneous polymer solution on a grid base, the grid base has a thickness of 50 μm, a pore diameter of 400 μm, and a line width of 50 μm, and the grid unit is a honeycomb through-hole membrane.
[0042] Step S3: Evaporate the solvent on the grid base with hot air, the temperature of the hot air is 22° C., the time of the hot air is 5 s, and the speed of the hot air is 3 m / s.
[0043] Step S4: After stopping the evaporation, a thin film is obtained.
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