A kind of active silicon antibacterial liquid modified by traditional Chinese medicine oil, its preparation method, and the preparation method of antibacterial coating
A technology of active silicon and antibacterial liquid, applied in the preparation of antibacterial coating, active silicon antibacterial liquid modified by traditional Chinese medicine oil and its preparation field, can solve the problems of rare antibacterial products, insufficient timeliness, unreachable, etc. Long-lasting bactericidal effect, long-lasting antibacterial effect, high-efficiency, best bactericidal effect
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Embodiment 1
[0041] The active silicon antibacterial liquid modified by traditional Chinese medicine oil is composed of: 15 parts of cinnamon essential oil, 15 parts of clove essential oil, 22 parts of N-β (aminoethyl)-γ-aminopropyltrimethoxysilane, 16 parts of 3-chloro -2-Hydroxypropyltrimethylammonium chloride, 7 parts of acetic acid, 3 parts of deionized water, 5 parts of zinc isooctanoate, 60 parts of ethyl acetate.
[0042] Prepare the antibacterial liquid according to the following steps: mix N-β(aminoethyl)-γ-aminopropyltrimethoxysilane, 3-chloro-2-hydroxypropyltrimethylammonium chloride, acetic acid, deionized water, iso Add zinc octanoate and ethyl acetate to the reaction kettle, heat to 80°C under stirring, and reflux for 2 hours, then add cinnamon essential oil and clove essential oil to the reaction kettle, keep the temperature constant, and continue stirring for 2 hours , after cooling.
[0043] The active silicon antibacterial liquid modified by traditional Chinese medicine ...
Embodiment 2
[0045] The active silicon antibacterial liquid modified by traditional Chinese medicine oil is composed of: 30 parts of forsythia oil, 10 parts of N-anilinomethyl triethoxysilane, 10 parts of 3-chloro-2-hydroxypropyl trimethyl bromide Ammonium, 20 parts of oxalic acid, 1 part of deionized water, 10 parts of dibutyltin dilaurate, 40 parts of methylal.
[0046] Prepare antibacterial liquid according to the following steps: N-anilinomethyltriethoxysilane, 3-chloro-2-hydroxypropyltrimethylammonium bromide, oxalic acid, deionized water, dibutyltin dilaurate, methylated Add the aldehyde into the reaction kettle, heat it to 60°C with stirring, and reflux for 1 hour, then add the forsythia oil into the reaction kettle, continue to stir and react for 3 hours, and then get the product after cooling.
[0047] The active silicon antibacterial liquid modified by traditional Chinese medicine oil was coated on the stainless steel surface to form a uniform coating, and then the coating was cu...
Embodiment 3
[0049] The active silicon antibacterial liquid modified by traditional Chinese medicine oil is composed of: 10 parts of wintergreen oil, 20 parts of N-anilinomethyltriethoxysilane, 20 parts of γ-aminoethylaminopropyltrimethoxysilane, 30 parts of Bis(dihydroxypropyl)dimethylammonium chloride, 1 part of formic acid, 10 parts of deionized water, 0.1 part of aluminum isopropoxide, 40 parts of isododecane, 40 parts of methylal.
[0050] Prepare antibacterial liquid according to the following steps: N-anilinomethyltriethoxysilane, γ-aminoethylaminopropyltrimethoxysilane, bis(dihydroxypropyl)dimethylammonium chloride, formic acid, Add ionized water, aluminum isopropoxide, isododecane, and methylal into the reactor, heat to 20°C under agitation, reflux for 3 hours, then add wintergreen oil into the reactor, and continue The reaction was stirred for 1 hour, and it was obtained after cooling.
[0051] The active silicon antibacterial liquid modified by traditional Chinese medicine oil ...
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