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Grating manufacturing process for adhering heavy metal colloid to light metal film

A production process and heavy metal technology, applied in the direction of diffraction grating, metal layered products, optics, etc., can solve the problems of high production cost, great influence of etching structure, complex process of photo-assisted electrochemical etching method, etc., and reach the production cycle Short, low cost and low price, convenient and fast production process

Active Publication Date: 2020-08-04
SHENZHEN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, in the process of research, it is found that when the grating 7 is made by this method, the grating 7 often breaks and collapses, which causes structural failure.
And the production cost is high, and the production area is small
[0005] The photo-assisted electrochemical etching method has a complicated process, and the silicon-based resistivity, temperature, etc. during the production process have a great influence on the etching structure, which is difficult to control. In the later stage of high atomic number metal filling process, all The required filling process is complex and the conditions are relatively harsh

Method used

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  • Grating manufacturing process for adhering heavy metal colloid to light metal film
  • Grating manufacturing process for adhering heavy metal colloid to light metal film
  • Grating manufacturing process for adhering heavy metal colloid to light metal film

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0056] Dissolve 30g of silver nitrate in 150mL of distilled water and 30mL of concentrated ammonia water to prepare a silver-ammonia complex solution; then dissolve 7.5g of lauric acid in 1000mL of distilled water and 75 mL of concentrated ammonia water to prepare an aqueous solution of lauric acid; turn on electric stirring The device mixes the silver ammonia solution and the lauric acid aqueous solution evenly, and controls the stirring speed at 800-1000 r / min. At room temperature, add NaBH4 solution dropwise to the above mixed solution, the molar ratio of reducing agent NaBH4 to silver nitrate is [AgNO3] / [NaBH4] = 4, and then stir for 1 h after the addition is completed, the black nano-silver Colloid; when it is necessary to prepare a large amount of nano-silver colloid, the amount of reagent can be increased in equal proportion.

[0057] In the present embodiment, when adding adhesive, adhesive is heating volatile adhesive; Adhesive includes bisphenol A type, novolac creso...

Embodiment 2

[0066] The sticky light metal film 1 is a long strip that has not been broken. The light metal film 1 is pre-cut into a piece of light metal film with a set shape and size, such as a light metal module with a length of 10 cm, a width of 6 cm, and a thickness of 30 microns; The width of the light metal is 6 cm, the thickness is 30 microns, and the thickness of the heavy metal layer 2 on the sticky light metal is 50 microns; the light metal film 1 is used as the bottom layer, and a layer of sticky light metal film 1 is covered on the light metal film 1, and then on the sticky light metal film 1 Stacking light metal films 1, stacking alternately to form a consistent film stack, the period of the grating 7 is 80 microns; among them, the alternate stacking adopts the zigzag stacking method, and the stacking efficiency is high; the opposite sides of the composite film stack will produce bending due to the sticky metal film resulting connection 13.

Embodiment 3

[0068] Both the light metal film 1 and the sticky light metal film 1 are broken into a metal film block of a set size, and one piece of light metal film is cut into one piece of light metal film with a set shape and size after passing through the rolling equipment, for example, the cut length is 10cm , an adhesive light metal module with a width of 6 cm and a thickness of 30 microns, the thickness of the heavy metal layer 2 on the adhesive light metal is 50 microns; the size of the light metal film 1 is exactly the same as that of the adhesive light metal; directly place the light metal film 1 and the adhesive metal module Stacked alternately to form a composite film stack; the period of the 7 gratings is 80 microns.

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Abstract

The invention belonging to the field of optical elements discloses a grating manufacturing process for adhering heavy metal colloid to a light metal film.. The process comprises the following five steps of preparing a heavy metal colloidal solution, adding an adhesive, adhering a heavy metal colloidal solution, manufacturing a composite film lamination, performing cutting and performing packaging.Firstly, heavy metal colloid is prepared through heavy metal salt; an adhesive which is easy to volatilize after being heated is added into the heavy metal colloid to increase the viscosity of the heavy metal colloid; a light metal film is adhered to the viscous heavy metal colloid to obtain two adhesive light metal films adhered with heavy metal layers, the light metal films and the adhesive light metal films are folded in a staggered manner to obtain a composite film stack, and finally the composite film stack is cut and packaged to obtain the grating. The whole grating preparation method is short in grating preparation period, low in cost and price and convenient and fast in preparation process. The manufactured structure cannot collapse, the grating with any area is manufactured by controlling the width of the light element metal plate, and the X-ray grating can be produced on a large scale through one-time manufacturing.

Description

technical field [0001] The invention relates to the technical field of optical elements, in particular to a grating manufacturing process in which a light metal film is adhered to a heavy metal colloid. Background technique [0002] X-ray imaging technology has developed rapidly as a brand-new subject since the discovery of X-ray by German researcher Roentgen in 1895. It can detect the internal defects of welds and equipment, and is widely used in machinery manufacturing, pressure vessels, aviation, etc. Aerospace, petroleum, chemical industry, railway transportation, metallurgy, shipbuilding, military and other industrial sectors; the current grating production process mainly uses DRIE technology, LIGA technology and silicon-based photo-assisted electrochemical etching technology. [0003] DRIE is an anisotropic dry etching technology, which is based on inductively coupled plasma for deep processing of silicon or other materials; firstly, the mask plate is covered on the su...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G02B5/18B32B15/01B32B7/12B32B37/12B32B43/00
CPCB32B7/12B32B15/01B32B37/1284B32B43/003G02B5/1847
Inventor 郭金川吴浩宗方轲杨君罗琨皓
Owner SHENZHEN UNIV
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