The application provides a core-shell heterogeneous gradient structure anti-
ionizing radiation powder and a preparation method and application thereof, and belongs to the field of
radiation protection. The preparation method of the core-shell heterogeneous gradient structure anti-
ionizing radiation powder comprises the following steps: adding a high-atomic-number
metal salt into deionized water, sequentially performing aging, washing,
drying and primary
calcination to obtain a core layer; adding the core layer and a low-atomic-number
metal salt into deionized water, sequentially performing aging, washing,
drying and primary
calcination to obtain a preliminary wrapped
powder in which a low-atomic-number
metal wraps a high-atomic-number metal core layer; adding the preliminary wrapped powder and a
rare earth salt into deionized water, sequentially performing aging, washing,
drying, primary
calcination, secondary calcination,
airflow pulverization and air rotation blowing to obtain the core-shell heterogeneous gradient structure anti-
ionizing radiation powder. Through the
synergy of the core-shell heterogeneous structure, high-atomic-number and low-atomic-number oxides and multiple
rare earth elements, the shielding performance of the material is significantly improved.