A kind of production device of mixed raw material high temperature resistant capacitive film for automobile and preparation process thereof
A technology of mixing raw materials and preparation processes, which is applied in the parts of fixed capacitors, the casing/package of fixed capacitors, laminated capacitors, etc., can solve the problems of poor film uniformity of film-forming capacitors, and achieve high cooling molding quality. , High economic benefit, stable film-forming performance
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Embodiment 1
[0046] A kind of mixed raw material high temperature resistant capacitor film for automobile and its preparation process
[0047] The high-temperature-resistant capacitor film of mixed raw materials for automobiles is prepared by the following process:
[0048] Step A, add flake graphite into potassium permanganate solution and mix, raise the temperature to 55°C, and stir for 15 hours; after the reaction, pour it into a hydrogen peroxide solution with a concentration of 28%, cool to room temperature, and then washing and drying in vacuum to obtain graphene oxide;
[0049] Step B, graphene oxide modification treatment: 4-nitrophthalonitrile, bisphthalonitrile, and copper acetate are mixed in a molar ratio of 6:2:1 to obtain a mixed solution, and graphene oxide is added to In ethanol, stir and mix evenly and ultrasonically oscillate for 20 minutes, then add the mixed solution, continue to stir and oscillate for 45 minutes, pour the obtained solution into a crystallization kettl...
Embodiment 2
[0057] A kind of mixed raw material high temperature resistant capacitor film for automobile and its preparation process
[0058] The high-temperature-resistant capacitor film of mixed raw materials for automobiles is prepared by the following process:
[0059] Step A, add flake graphite into potassium permanganate solution and mix, raise the temperature to 55°C, and stir for 15 hours; after the reaction, pour it into a hydrogen peroxide solution with a concentration of 28%, cool to room temperature, and then washing and drying in vacuum to obtain graphene oxide;
[0060] Step B, graphene oxide modification treatment: 4-nitrophthalonitrile, bisphthalonitrile, and copper acetate are mixed in a molar ratio of 5:2:1 to obtain a mixed solution; graphene oxide is added to In ethanol, stir and mix evenly and ultrasonically oscillate for 20 minutes, then add the mixed solution, and continue to stir and oscillate for 45 minutes; pour the obtained solution into a crystallization kettl...
Embodiment 3
[0068] A kind of mixed raw material high temperature resistant capacitor film for automobile and its preparation process
[0069] The high-temperature-resistant capacitor film of mixed raw materials for automobiles is prepared by the following process:
[0070] Step A, add flake graphite into potassium permanganate solution and mix, raise the temperature to 55°C, and stir for 15 hours; after the reaction, pour it into a hydrogen peroxide solution with a concentration of 28%, cool to room temperature, and then washing and drying in vacuum to obtain graphene oxide;
[0071] Step B, graphene oxide modification treatment: 4-nitrophthalonitrile, bisphthalonitrile, and copper acetate are mixed in a molar ratio of 7:2:1 to obtain a mixed solution; graphene oxide is added to In ethanol, stir and mix evenly and ultrasonically oscillate for 20 minutes, then add the mixed solution, continue to stir and oscillate for 45 minutes; pour the obtained solution into a crystallization kettle at...
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