Colored dry-mixed mortar and preparation method thereof
A dry-mixed mortar and color technology, applied in the field of titanium dioxide, can solve the problems of poor weather resistance, pan-alkali, etc., and achieve the effect of enhancing vividness and strong heating capacity
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Embodiment 1
[0095] To prepare colored dry mix mortar:
[0096] (1) Preparation of modified titanium dioxide:
[0097] Raw materials (by weight): 1 part of butyl titanate, 10 parts of water;
[0098] A1. Add butyl titanate into the reactor, at a temperature of 85°C, N 2 Gasification of butyl titanate under protection;
[0099] A2. Add water into the reactor; the reaction temperature is 525°C and the pressure is 1.01×10 5 Pa, N 2 Reaction under the protection of (nitrogen flow rate 1L / min, water vapor flow rate 1L / min, reaction time 30min) to obtain R818 type nano-TiO 2 ;
[0100] A3. The nano-TiO obtained in step A2 2 placed under inert gas CO 2 Cool down to 23°C in the atmosphere;
[0101] A4. The TiO obtained by cooling in step A3 2 Placed in a 45μm round-hole sieve to control TiO 2 The content is greater than 98%, the sieve residue is less than 0.01%, the volatile matter at 105°C is less than 0.05%, and the L value ranges from 98.5 to 100 to obtain the finished product of modi...
Embodiment 2
[0121] To prepare colored dry mix mortar:
[0122] (1) Preparation of modified titanium dioxide:
[0123] Raw materials (by weight): 1 part of butyl titanate, 15 parts of water;
[0124] A1. Add butyl titanate into the reactor, at a temperature of 60°C, N 2 Gasification of butyl titanate under protection;
[0125] A2. Add water into the reactor; the reaction temperature is 510°C and the pressure is 1.5×10 5 Pa, N 2 Reaction under the protection of (nitrogen flow rate 1L / min, water vapor flow rate 1L / min, reaction time 30min) to obtain R818 type nano-TiO 2 ;
[0126] A3. The nano-TiO obtained in step A2 2 placed under inert gas CO 2 Cool down to 22°C in the atmosphere;
[0127] A4. The TiO obtained by cooling in step A3 2 Placed in a 45μm round-hole sieve to control TiO 2 The content is greater than 98%, the sieve residue is less than 0.01%, the volatile matter at 105°C is less than 0.05%, and the L value ranges from 98.5 to 100 to obtain the finished product of modif...
Embodiment 3
[0147] To prepare colored dry mix mortar:
[0148] (1) Preparation of modified titanium dioxide:
[0149] Raw materials (by weight): 1 part of butyl titanate, 6 parts of water;
[0150] A1. Add butyl titanate into the reactor, at a temperature of 110°C, N 2 Gasification of butyl titanate under protection;
[0151] A2. Add water into the reactor; the reaction temperature is 530°C and the pressure is 0.5×10 5 Pa, N 2 Reaction under the protection of (nitrogen flow rate 1L / min, water vapor flow rate 1L / min, reaction time 20min) to obtain R818 type nano-TiO 2 ;
[0152] A3. The nano-TiO obtained in step A2 2 placed under inert gas CO 2 Cool down to 24°C in the atmosphere;
[0153] A4. The TiO obtained by cooling in step A3 2 Placed in a 45μm round-hole sieve to control TiO 2 The content is greater than 98%, the sieve residue is less than 0.01%, the volatile matter at 105°C is less than 0.05%, and the L value ranges from 98.5 to 100 to obtain the finished product of modif...
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