Preparation method of titanium carbide hollow spheres
A technology of titanium carbide and hollow spheres is applied in the direction of titanium carbide and carbide, which can solve the problems of complex preparation process and achieve the effect of simple synthesis.
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[0031] Example 1
[0032] Pour 40 mL of 9 M hydrochloric acid solution into a polytetrafluoroethylene beaker and start stirring, then add 2 g of lithium fluoride and continue stirring at room temperature for 30 minutes; add 2 g of Ti 3 AlC 2 The powder was slowly added to the above solution, and then continuously stirred and reacted at 35°C for 24 hours. The corrosion products are then centrifuged, and the supernatant is discarded. Then wash with deionized water by centrifugation for 6 times until the pH of the supernatant is 6; use anhydrous ethanol for 2 hours to intercalate the precipitate after centrifugation, and then centrifuge to pour out the ethanol. Then add deionized water to the sediment after the first centrifugation. After ultrasonic stripping, take the suspension again after centrifugation. Then add deionized water for ultrasonic stripping and then centrifuge to get the suspension. Take 5 times to get a small layer of titanium carbide nano Tablet dispersion. Dilut...
Example Embodiment
[0034] Example 2
[0035] Take 20 mL of 9 M hydrochloric acid solution into a polytetrafluoroethylene beaker and start stirring, then add 2 g of lithium fluoride and continue stirring at room temperature for 30 minutes; add 2 g of Ti 3 AlC 2 The powder was slowly added to the above solution, and then continuously stirred and reacted at 35°C for 24 hours. The corrosion products are then centrifuged, and the supernatant is discarded. Then centrifuge with deionized water to wash 5 times until the pH of the supernatant is 6; sonicate the precipitate after the centrifugation with absolute ethanol for 1 hour to intercalate, and then centrifuge to discard the ethanol. Then add deionized water to the sediment after the first centrifugation. After ultrasonic stripping, take the suspension again after centrifugation. Then add deionized water for ultrasonic stripping and then centrifuge to get the suspension. Take 5 times to get a small layer of titanium carbide nano Tablet dispersion. Di...
Example Embodiment
[0037] Example 3
[0038] Take 60 mL of 12 M hydrochloric acid solution into a polytetrafluoroethylene beaker and start stirring, then add 1 g of lithium fluoride and continue stirring at room temperature for 60 minutes; add 0.5 g of Ti 3 AlC 2 The powder was slowly added to the above solution, and then continuously stirred at 35°C for 24 hours. The corrosion products are then centrifuged, and the supernatant is discarded. Then centrifuged with deionized water to wash 5 times until the pH of the supernatant was 6; ultrasonicated with absolute ethanol for 1.5 hours to intercalate the precipitate after centrifugation, and then centrifuged to discard the ethanol. Then add deionized water to the sediment after the first centrifugation. After ultrasonic stripping, take the suspension again after centrifugation, add deionized water for ultrasonic stripping and then centrifuge to get the suspension. Take 8 times to get the few layers of titanium carbide nano Tablet dispersion. Dilute ...
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