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Anti-bacterial nanofiber material and application thereof

A nanofiber, antibacterial technology, applied in the field of antibacterial nanofiber materials, can solve the problems of reducing the mechanical properties of fibers, easy to block needles, easy to fall off, etc., to achieve good washing resistance, improved mechanical properties, and good antibacterial effect. Effect

Inactive Publication Date: 2020-11-27
嘉兴市爵拓科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In the process of adding titanium dioxide nanoparticles to the spinning solution for electrospinning to obtain antibacterial fibers, titanium dioxide nanoparticles are easy to form agglomerates and easily block the needle, making the antibacterial effect worse, and the durability of titanium dioxide nanoparticle-loaded fibers is the same. Poor, titanium dioxide nanoparticles are easy to fall off during washing and friction, which affects the antibacterial effect, and when adding titanium dioxide nanoparticles to the spinning solution to prepare antibacterial fibers, knots will be formed in the fibers, reducing the mechanical properties of the fibers

Method used

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  • Anti-bacterial nanofiber material and application thereof
  • Anti-bacterial nanofiber material and application thereof
  • Anti-bacterial nanofiber material and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] A kind of preparation method of antibacterial nanofiber,

[0026] Modification of titanium dioxide nanoparticles: ultrasonically disperse titanium dioxide nanoparticles in absolute ethanol to obtain a titanium dioxide nanoparticle dispersion, add polydipside, stir and disperse for 1 hour to obtain a polydipside / titanium dioxide mixed solution; add water to the mixture under stirring, and filter with suction. , the filter cake was re-dispersed in water and stirred for 1 h, and the suction filtration and washing were repeated twice; after drying at 25 °C, the titanium dioxide pretreated powder was obtained after ball milling with a ball mill for 12 h; the titanium dioxide pretreated powder was placed in a crucible, and the Modified titanium dioxide was prepared after calcining in a Furnace for 4 hours; the mass fraction of the titanium dioxide nanoparticle dispersion was 4wt%, the addition amount of polydipside was 160wt% of the titanium dioxide nanoparticle, and the addit...

Embodiment 2

[0030] A kind of preparation method of antibacterial nanofiber,

[0031]Modification of titanium dioxide nanoparticles: ultrasonically disperse titanium dioxide nanoparticles in absolute ethanol to obtain a titanium dioxide nanoparticle dispersion, add polydipside, stir and disperse for 1 hour to obtain a polydipside / titanium dioxide mixed solution; add water to the mixture under stirring, and filter with suction. , the filter cake was redispersed in water and stirred for 1 h, and the suction filtration and washing were repeated twice; after drying at 25 °C, the titanium dioxide pretreated powder was obtained after ball milling with a ball mill for 12 h; the titanium dioxide pretreated powder was placed in a crucible, and the Modified titanium dioxide was prepared after calcining in a Furnace for 4 hours; the mass fraction of the titanium dioxide nanoparticle dispersion was 4wt%, the addition amount of polygoside was 300wt% of the titanium dioxide nanoparticle, and the addition...

Embodiment 3

[0035] A kind of preparation method of antibacterial nanofiber,

[0036] Modification of titanium dioxide nanoparticles: ultrasonically disperse titanium dioxide nanoparticles in absolute ethanol to obtain a titanium dioxide nanoparticle dispersion, add polydipside, stir and disperse for 1 hour to obtain a polydipside / titanium dioxide mixed solution; add water to the mixture under stirring, and filter with suction. , the filter cake was redispersed in water and stirred for 1 h, and the suction filtration and washing were repeated twice; after drying at 25 °C, the titanium dioxide pretreated powder was obtained after ball milling with a ball mill for 12 h; the titanium dioxide pretreated powder was placed in a crucible, and the Modified titanium dioxide was prepared after calcining in a Furnace for 4 hours; the mass fraction of the titanium dioxide nanoparticle dispersion was 4wt%, the addition amount of polygoside was 300wt% of the titanium dioxide nanoparticle, and the additio...

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PUM

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Abstract

The invention discloses an anti-bacterial nanofiber material and application thereof, and belongs to the technical field of nanofiber materials. The anti-bacterial nanofiber material is prepared by performing electrostatic spinning on a spinning solution containing modified titanium dioxide nanoparticles, wherein a preparation method for the modified titanium dioxide nanofiber material comprises the following steps of uniformly mixing polydatin and a titanium dioxide nanoparticle dispersion liquid; and adding water with stirring, and performing suction filtration, washing, ball milling with aball mill and calcining to obtain the modified titanium dioxide nanoparticles. According to the anti-bacterial nanofiber material prepared by from the modified titanium dioxide nanoparticles, PET andPA6, the anti-bacterial performance is at least up to 90 percent, and the antibacterial ratio is reduced by less than 1 percent after washing by 50 times.

Description

technical field [0001] The invention belongs to the technical field of nanofiber materials, and in particular relates to an antibacterial nanofiber material and uses thereof. Background technique [0002] Antibacterial fiber refers to a new type of functional fiber that can kill or inhibit microorganisms. It is now widely used in home textiles (including underwear, sweatshirts, old, pregnant and infant clothing, etc.) and medical textiles (surgical gowns, hospital gowns, bed sheets, etc.). , curtains, and bandages, etc.). Fabrics made of antibacterial fibers can resist the adhesion of bacteria on the fabric, reduce the number of bacteria on the fabric, ensure the safety of people-fabric-environment, and keep people away from germs. The earliest use of the concept of antibacterial by humans can be traced back to the Neolithic Age more than 10,000 years ago, when people began to use salt to preserve food for long-term storage, and salt became the earliest antiseptic and antib...

Claims

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Application Information

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IPC IPC(8): D01F8/14D01F8/12D01F1/10D01D5/00B82Y40/00
CPCB82Y40/00D01D5/003D01F1/10D01F1/103D01F8/12D01F8/14
Inventor 不公告发明人
Owner 嘉兴市爵拓科技有限公司
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