Nano-diamond cutter and preparation method and application thereof
A technology of nano-diamond and diamond tools, which is applied in metal processing equipment, manufacturing tools, welding equipment, etc., and can solve problems such as difficult welding and difficult preparation of diamond tools
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Embodiment 1
[0069] This example provides a kind of preparation method of nano-diamond cutting tool, and it comprises the steps:
[0070] (1) Pretreatment process: 5mm square CVD single crystal diamond
[0071] Stress microscope inspection: check that there is more stress inside the diamond, and the stress is less;
[0072] X-ray transmission inspection: no cracks or holes inside the diamond;
[0073] Heat treatment: high-purity nitrogen (99.99%), 650°C, 10h;
[0074] Cold treatment: no;
[0075] Heat treatment: no;
[0076] (2) Cutting and shaping process: laser directional cutting (the power of the laser cutting is 500W, the wavelength is 192nm), and four 2.5mm square diamond single crystal substrates are obtained;
[0077] (3) Polishing process:
[0078] Matrix orientation: X-ray diffraction orientation;
[0079] Substrate fixation: take (100) crystal face grinding, use silver brazing, welding in argon protective atmosphere, welding temperature 450-600 ℃;
[0080] Substrate polis...
Embodiment 2
[0090] This example provides a kind of preparation method of nano-diamond cutting tool, and it comprises the steps:
[0091] (1) Pretreatment process: irregular high temperature and high pressure single crystal diamond with a diameter of 5 mm;
[0092] Stress microscope inspection: check that there are a large number of irregular stress layers inside the diamond, and the stress is relatively large;
[0093] X-ray transmission inspection: there are cracks on the surface and inside, and there are a large number of uneven nanometer to micrometer holes inside;
[0094] Heat treatment: high-purity nitrogen (99.99%), 650°C, 10h;
[0095] Cold treatment: liquid nitrogen (minus 196°C), treatment for 5 hours;
[0096] Hot pressing treatment: 130MPa, 180℃, 10h;
[0097] (2) Cutting and shaping process: laser directional cutting (the power of the laser cutting is 1kW, the wavelength is 512nm), 1 piece of 2.5mm irregular single crystal substrate, 3 pieces of 0.2-0.5mm irregular single ...
Embodiment 3
[0111] This example provides a kind of preparation method of nano-diamond cutting tool, and it comprises the steps:
[0112] (1) Pretreatment process: irregular natural single crystal diamond with a diameter of 5mm;
[0113] Stress microscope inspection: check that there are a large number of irregular stress layers inside the diamond, and the stress is relatively large;
[0114] X-ray transmission inspection: there are cracks on the surface and inside;
[0115] Heat treatment: high-purity nitrogen (99.99%), 650°C, 10h;
[0116] Cold treatment: no;
[0117] Hot pressing treatment: 130MPa, 180℃, 10h;
[0118] (2) Cutting and shaping process: laser directional cutting (the power of the laser cutting is 2kW, the wavelength is 1190nm), to obtain 2 pieces of 2.5mm irregular single crystal substrates, and 2 pieces of 0.2-0.5mm irregular single crystal substrates;
[0119] (3) Polishing process:
[0120] Matrix orientation: X-ray diffraction orientation;
[0121] Substrate fixa...
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