A kind of novel catalyst material and its preparation method and application
A catalytic material and solvothermal reaction technology, applied in chemical instruments and methods, oxidized water/sewage treatment, electrolytic components, etc., can solve the problems of restricting large-scale use, high cost and scarcity, and achieve large-scale production, The effect of reducing secondary pollution and excellent performance of hydrogen and oxygen production
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[0051] CoNi-MOFs / S-g-C 3 N 4 The preparation method of electrode, comprises the steps:
[0052] (1) 1.8mmol Co(NO 3 ) 2 , 0.5mmol Ni(NO 3 ) 2 , 4 mmol NH 4 F and 10mmol CH 4 N 2 O (urea) is dissolved in 40mL deionized water and makes reaction solution;
[0053] Place nickel foam in a reaction solution at 120°C for solvothermal reaction for 5 hours, cool to room temperature after the reaction is completed, wash with deionized water, and dry in vacuum to obtain a precursor electrode containing Co and Ni elements;
[0054] (2) Place the imidazole and the precursor electrode prepared in (1) at both ends of the quartz tube, the imidazole end is placed near the gas flow inlet, and the precursor electrode is placed near the gas flow outlet, and then calcined at 300 ° C under nitrogen atmosphere , get CoNi-MOFs electrode;
[0055] (3) Dissolve melamine (10mmol) and thiocyanic acid (10mmol) in 50.0mL distilled water and 50.0mL N,N dimethylformamide respectively at 80°C. After...
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