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Processing method of inorganic copper preparation

A processing method and inorganic copper technology, applied in botany equipment and methods, chemicals for biological control, biocides, etc., can solve problems such as prone to phytotoxicity, uneven particle size distribution, and poor mixing of liquid medicines , to achieve the effect of improving equipment utilization rate and production efficiency, improving mixing suitability, and meeting market supply

Inactive Publication Date: 2021-04-06
JIANGXI HEYI CHEM
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Because the use of domestic inorganic copper preparations is prone to phytotoxicity and poor mixing, the phenomenon of "copper fear" is common.
[0004] At present, the domestic production process of wettable powder, water dispersible granule, and water suspension concentrate of inorganic copper preparations is mostly one-step mixing and pulverization or multiple airflow pulverization after mixing evenly, that is, the active ingredients containing inorganic copper and surfactants, After the medium is mixed evenly, the finished product is obtained after airflow crushing or wet sand milling to reach a certain particle size. The disadvantage is that the production efficiency is low, it is difficult to obtain a finished product with a small particle size, and the particle size distribution of the obtained product is wide.
The particle size distribution of the product is uneven, resulting in a low suspension rate and easy aggregation and precipitation of the product, resulting in uneven drug use on the target, poor mixing of the drug solution and phytotoxicity

Method used

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  • Processing method of inorganic copper preparation
  • Processing method of inorganic copper preparation

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] 1. Production of 50% king copper wettable powder

[0032] Take 98% of the original copper king, adopt 600 type jet crushing, control the crushed king copper powder D97 to be less than 25 microns, and obtain 98% king copper powder after collection;

[0033] Select 98% king copper former powder 510Kg and tensio-active agent D8818 40Kg, WLNOK-K 40Kg, white carbon black 30Kg, kaolin 380Kg, through airflow pulverization after fully uniform mixing, control particle diameter D97 to be less than 10 microns, obtain finished product; The analysis of the finished product shows that the suspension rate reaches 93%, and it has better compatibility with other preparations; the pulverization time is narrower than that of the original one-step method to obtain the same particle size powder, and the pulverization time can be shortened by more than half.

Embodiment 2

[0035] 2. Production of 30% King Copper Water Suspension Concentrate

[0036] Get 98% king copper former medicine, adopt 600 type jet milling, the king copper former powder D97 after controlling pulverization is less than 25 microns, obtain 98% king copper former powder after collecting;

[0037] Select 310Kg of 98% king copper raw powder, 40Kg of surfactant FS3000, 1g of magnesium aluminum silicate, 2Kg of xanthan gum, 50Kg of ethylene glycol, 2Kg of defoamer, 2Kg of preservative, and 584Kg of deionized water. Wet pulverization of the mill, the particle size D97 is controlled to be less than 4 microns, and the finished product is obtained; after the analysis of the finished product, the suspension rate reaches 98%, and the compatibility with other preparations is better; the pulverization time is longer than that of the original one-step method to obtain the same particle size The diameter powder distribution is narrower, and the crushing time can be shortened by more than ha...

Embodiment 3

[0039] 3. Production of 86.2% cuprous oxide wettable powder

[0040] Take 98% cuprous oxide former medicine, adopt 600 type jet milling, control the king copper former powder D97 after pulverizing to be less than 15 microns, obtain 98% cuprous oxide former powder after collecting;

[0041] Select 98% cuprous oxide raw powder 880Kg and surfactant D8818 40Kg, WLNOK-K 40Kg, white carbon black 30Kg, kaolin 10Kg, after fully and evenly mixed, through jet pulverization, control particle diameter D97 to be less than 5 microns, obtain finished product; The analysis of the finished product shows that the suspension rate reaches 90%, and it has better compatibility with other preparations; the pulverization time is narrower than that of the original one-step method to obtain the same particle size powder, and the pulverization time can be shortened by more than half.

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Abstract

The invention aims to provide a processing method of an inorganic copper preparation, which comprises the following steps: (1) adding an inorganic copper raw medicine into a premixer, mixing for 30 minutes, setting the rotating speed of a grading wheel motor of a crushing main machine to be not less than 4000 revolutions per minute, starting an airflow crushing induced draft fan, opening an air inlet valve of the main machine, controlling the pressure of compressed airflow to be not less than 0.8 Mpa, opening a feeding valve to enable the materials to pass through a jet mill at a constant speed, and performing jet milling through classification to obtain pretreated materials with the particle size D97 of less than 25 microns. According to the present invention, the pretreatment work of the effective components of the inorganic copper-containing preparation can be prepared in advance in the slack season during the production, the batch production can be rapidly achieved during the post-mixing crushing, and the equipment utilization rate and the production efficiency are improved to meet market supply; 2, enabling the product produced by adopting the new process to have narrow particle size distribution, so that the product with high suspension rate can be obtained more easily; and 3, greatly improving the mixing suitability of the product produced by adopting the new process.

Description

technical field [0001] The invention relates to an inorganic copper preparation, in particular to a processing method of the inorganic copper preparation. Background technique [0002] Inorganic copper preparations are the top-ranked fungicides in the world, with annual sales of more than 600 million US dollars, and have been used worldwide for more than 100 years. From the perspective of the international market, as the first commercialized pesticide variety, the application of copper preparations has been very stable. Due to its excellent dual killing effect on fungi and bacteria, it has occupied a leading position in the international market for a long time. [0003] However, it is such a broad-spectrum, low-cost, and non-resistant fungicide that has been in a tepid situation in China for a long time. Due to the use of domestic inorganic copper preparations, the phenomenon of "copper fear" such as phytotoxicity and poor mixing performance is common. [0004] At present,...

Claims

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Application Information

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IPC IPC(8): A01N59/20A01N25/14A01N25/04A01P1/00A01P3/00
CPCA01N25/04A01N25/14A01N59/20
Inventor 冯亚东詹敏敏杨的妹严强欧阳灿柴明根马超王光瀛贾志新
Owner JIANGXI HEYI CHEM
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