Well cementation composite plugging spacer fluid system and application thereof
A technology of isolation fluid and system, applied in the field of petroleum exploration, can solve the problem of ineffective plugging effect of cavities or broken formations, etc.
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[0064] Preparation method of raw material:
[0065] 1. Preparation method of polyethylene temperature-sensitive expansion material with a temperature-sensitive point of 150°C
[0066] Mix 50mL of liquid paraffin with 3mL of compound emulsifier, stir at room temperature until the emulsifier and oil-soluble solvent are completely mixed to form an oil phase; put 0.5g of polyvinyl alcohol and 1g of N-isopropylacrylamide into 10mL of deionized water, and Stir for 10 minutes until the polyvinyl alcohol and N-isopropylacrylamide are completely dissolved, add 0.25mL hydrochloric acid and 0.25mL glutaraldehyde to form a water phase; slowly drop the water phase into the oil phase under stirring at room temperature, and stir for 10 minutes to reach the water phase Evenly dispersed in the oil phase. After heating at 150°C for 30min, slowly add 0.1mL tetraethylenepentamine dropwise to the oil phase, then add 0.04g dibenzoyl peroxide, continue to react for 3h, centrifuge after reaction, wa...
Embodiment 1
[0078] (1) Weigh 500g of fresh water, 15g of polyethylene temperature-sensitive swelling fine particles (the temperature-sensitive point of the particles is 150°C, the mesh size is 4-400 mesh), 7.5g of polyethylene temperature-sensitive swelling fibers (the temperature-sensitive point of the fibers is 150°C, the length 0.05-10cm, diameter 5-300μm), polypropylene microfiber 1.5g, weighting agent 300g, high temperature suspension stabilizer 50g, high temperature retarder 5g, defoamer 1.5g.
[0079] (2) Mixing the weighed temperature-sensitive expandable fine particles, temperature-sensitive expandable fibers, fine fibers and weighting agent uniformly to obtain a mixed powder.
[0080] (3) Mix the weighed fresh water, high-temperature suspension stabilizer, high-temperature retarder and defoamer evenly to obtain a mixed liquid.
[0081] (4) In the mixing container, add the mixed liquid, the agitator rotates at a low speed (4000±200 rpm), and within 15 seconds, the mixture is even...
Embodiment 2-3
[0083] The only difference from Example 1 is that the content of the slag weighting agent used is 475g and 725g respectively, and the obtained density is respectively 1.40g / cm 3 and 1.50g / cm 3 The cementing composite plugging spacer fluid system.
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