Self-cleaning antibacterial non-woven fabric and preparation method thereof
A non-woven fabric, self-cleaning technology, applied in textiles and papermaking, biochemical fiber treatment, fiber type, etc., can solve the problem of non-active groups on the surface of polypropylene non-woven fabrics, and achieve excellent antibacterial properties
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Embodiment 1
[0022] A kind of self-cleaning antibacterial non-woven fabric, its preparation method comprises the steps:
[0023] S1, the polypropylene non-woven fabric (30g / m 2 ) was cut into a size of 10cm×5cm, ultrasonically treated in ethanol for 30min to remove surface dust, rinsed repeatedly with deionized water and then dried for later use; adding dopamine hydrochloride into Tris buffer (pH=8.5) and stirring Dissolve, be configured into the solution that concentration is 30mmol / L, then add ammonium persulfate and ethylenediamine equimolar with dopamine hydrochloride, obtain dopamine solution; With above-mentioned polypropylene nonwoven fabric according to bath ratio (g / mL) 1: 40 soaked in the above-mentioned dopamine solution, shaken and reacted in a constant temperature water bath shaker at 25°C for 2 hours, then took it out, rinsed with deionized water, and dried to obtain a non-woven fabric with a polydopamine layer adhered to the surface;
[0024] S2, chitosan (deacetylation deg...
Embodiment 2
[0027] A kind of self-cleaning antibacterial non-woven fabric, its preparation method comprises the steps:
[0028] S1, the polypropylene non-woven fabric (30g / m 2 ) was cut into a size of 10cm×5cm, ultrasonically treated in ethanol for 30min to remove surface dust, rinsed repeatedly with deionized water and then dried for later use; adding dopamine hydrochloride into Tris buffer (pH=8.5) and stirring Dissolve and configure a solution with a concentration of 30mmol / L, then add ammonium persulfate with 2 times the molar quantity of dopamine hydrochloride and ethylenediamine with 3 times the molar quantity of dopamine hydrochloride to obtain a dopamine solution; (g / mL) 1:40 Soak in the above dopamine solution, shake and react in a constant temperature water bath shaker at 25°C for 1 hour, take it out, rinse with deionized water, and dry to obtain a non-woven fabric with a polydopamine layer adhered to the surface;
[0029] S2, chitosan (deacetylation degree ≥ 80%) is added in t...
Embodiment 3
[0032] A kind of self-cleaning antibacterial non-woven fabric, its preparation method comprises the steps:
[0033] S1, the polypropylene non-woven fabric (30g / m 2 ) was cut into a size of 10cm×5cm, ultrasonically treated in ethanol for 30min to remove surface dust, rinsed repeatedly with deionized water and then dried for later use; adding dopamine hydrochloride into Tris buffer (pH=8.5) and stirring Dissolve and configure a solution with a concentration of 30mmol / L, then add ammonium persulfate of 3 times the molar amount of dopamine hydrochloride and ethylenediamine of 4 times the molar amount of dopamine hydrochloride to obtain a dopamine solution; (g / mL) 1:40 soaked in the above-mentioned dopamine solution, shaken and reacted in a constant temperature water bath shaker at 25°C for 3 hours, took it out, rinsed with deionized water, and dried to obtain a non-woven fabric with a polydopamine layer adhered to the surface;
[0034] S2, chitosan (deacetylation degree ≥ 80%) is...
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