Cement-based waterproof material and preparation process thereof
A waterproof material, cement-based technology, applied in the field of waterproof materials, can solve the problems of low bonding strength and flexibility, short initial setting time, etc.
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[0025] In one embodiment of the present invention, the sulfonated SBS has a sulfonation degree of 8-16%, wherein the mass content of styrene is 30-45%; and the number average molecular weight is 50000-80000. In one embodiment of the present invention, the 2-acrylamido-2-methylpropanesulfonic acid / N-trimethylolmethacrylamide / aluminum acrylate / vinyltriethoxysilane / 3,5- The preparation method of diamino-1H-pyrazole-4-carboxylic acid allyl ester copolymer comprises the steps of: combining 2-acrylamido-2-methylpropanesulfonic acid, N-trimethylolmethacrylamide , Vinyltriethoxysilane, allyl 3,5-diamino-1H-pyrazole-4-carboxylate, and initiator are added to the high boiling point solvent, and the reaction is stirred at 65-75°C in an inert gas atmosphere After 4-6 hours, the solvent was removed by rotary evaporation to obtain 2-acrylamido-2-methylpropanesulfonic acid / N-trimethylolmethacrylamide / vinyl triethoxysilane / 3,5-di Allyl amino-1H-pyrazole-4-carboxylate copolymer.
[0026] In o...
Embodiment 1
[0037] A cement-based waterproof material, characterized in that it includes the following components in parts by weight: 30 parts of cement, 15 parts of pozzolan, 1 part of fluorogypsum, 4 parts of hydrophilic nitrogen-doped carbon nanofibers, hyperbranched 4A 2 parts of molecular sieve, 1 part of epoxy-based organic fluorosilicone oil, 5 parts of sulfonated SBS, 3 parts of hyperbranched sulfonate surfactant SHBP-1, 2-acrylamido-2-methylpropanesulfonic acid / N-tri 8 parts of methylolmethacrylamide / vinyltriethoxysilane / 3,5-diamino-1H-pyrazole-4-carboxylate allyl ester copolymer, 0.1 part of aluminum acrylate, 0.1 part of water-soluble initiator parts, 20 parts of water.
[0038] The cement is ordinary Portland 42.5 cement; the particle diameter of the pozzolan is 300 mesh; the particle diameter of the fluorogypsum is 500 mesh; the sulfonation degree of the sulfonated SBS is 8%, wherein the mass of styrene The content is 30%; the number average molecular weight is 50000.
[00...
Embodiment 2
[0042] A cement-based waterproof material, characterized in that it comprises the following components in parts by weight: 33 parts of cement, 17 parts of pozzolan, 1.5 parts of fluorogypsum, 5 parts of hydrophilic nitrogen-doped carbon nanofibers, hyperbranched 4A 2.5 parts of molecular sieve, 1.5 parts of epoxy-based organofluorosilicone oil, 6 parts of sulfonated SBS, 3.5 parts of hyperbranched sulfonate surfactant SHBP-1, 2-acrylamido-2-methylpropanesulfonic acid / N-tri 9 parts of methylolmethacrylamide / vinyltriethoxysilane / 3,5-diamino-1H-pyrazole-4-carboxylate allyl ester copolymer, 0.15 parts of aluminum acrylate, 0.13 parts of water-soluble initiator part, 23 parts of water; the cement is ordinary Portland 42.5R cement; the particle diameter of the pozzolan is 400 mesh; the particle diameter of the fluorogypsum is 600 mesh; the sulfonation degree of the sulfonated SBS is 10 %, wherein the mass content of styrene is 33%; the number average molecular weight is 60000.
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